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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
3162-52-5
合成路线
（共 9 条）
7499-99-2
+
100-44-7
苄基氯
→
反应条件
3162-52-5
反应条件
potassium carbonate; acetone
参考文献
Rabjohn; Rosenburg
Journal of Organic Chemistry, 1959 , vol. 24, p. 1192,1195
Full Text Show Details
Geissman
Journal of the American Chemical Society, 1951 , vol. 73, p. 3514
6274-74-4
+
75-36-5
乙酰氯
→
反应条件
3162-52-5
反应条件
aluminium trichloride; benzene
参考文献
Geissman
Journal of the American Chemical Society, 1951 , vol. 73, p. 3514
7499-99-2
→
反应条件
3162-52-5
反应条件
1: K2CO3 / dimethylformamide / 0.17 h / 150 °C 2: 100 percent / conc. HCl, acetic acid / 1 h / Ambient temperature View Scheme
参考文献
Horie, Tokunaru; Shibata, Kenichi; Yamashita, Kazuyo; Kawamura, Yasuhiko; Tsukayama, Masao
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 3 p. 446 - 451
100-44-7
苄基氯
→
反应条件
3162-52-5
反应条件
1: K2CO3 / dimethylformamide / 0.17 h / 150 °C 2: 100 percent / conc. HCl, acetic acid / 1 h / Ambient temperature View Scheme
参考文献
Horie, Tokunaru; Shibata, Kenichi; Yamashita, Kazuyo; Kawamura, Yasuhiko; Tsukayama, Masao
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 3 p. 446 - 451
3162-52-5
→
反应条件
35214-88-1
反应条件
1: 83 percent / K2CO3, KI / acetone; dimethylformamide / Heating 2: 75 percent / AlBr3, NaI / acetonitrile / 0.25 h / 0 °C 3: pyridine / 2 h / 70 - 80 °C 4: KOH / pyridine / 80 °C 5: 87 percent / conc. H2SO4, acetic acid / 1 h / 50 °C 6: 71 percent / dimethyldioxirane / acetone / 0 °C 7: 96 percent / K2CO3 / acetone / Heating 8: 91 percent / AlCl3 / acetonitrile / 0.5 h / Ambient temperature 9: 90 percent / K2CO3 / methanol / 1.5 h / Heating 10: 90 percent / H2 / 10percent Pd/C / methanol; ethyl acetate / Ambient temperature View Scheme
参考文献
Horie, Tokunaru; Shibata, Kenichi; Yamashita, Kazuyo; Kawamura, Yasuhiko; Tsukayama, Masao
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 3 p. 446 - 451
3162-52-5
→
反应条件
3153-83-1
反应条件
1: 83 percent / K2CO3, KI / acetone; dimethylformamide / Heating 2: 75 percent / AlBr3, NaI / acetonitrile / 0.25 h / 0 °C 3: pyridine / 2 h / 70 - 80 °C 4: KOH / pyridine / 80 °C 5: 97 percent / conc. H2SO4, acetic acid / 1 h / 50 °C 6: 56 percent / dimethyldioxirane / acetone / 0 °C 7: 98 percent / K2CO3 / acetone / Heating 8: 85 percent / AlCl3 / acetonitrile / 0.5 h / Ambient temperature 9: 85 percent / K2CO3 / methanol / 1.5 h / Heating 10: 76 percent / H2 / 10percent Pd/C / methanol; ethyl acetate / Ambient temperature View Scheme
参考文献
Horie, Tokunaru; Shibata, Kenichi; Yamashita, Kazuyo; Kawamura, Yasuhiko; Tsukayama, Masao
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 3 p. 446 - 451
3162-52-5
→
反应条件
32520-55-1
6-甲氧基山柰酚
反应条件
1: 83 percent / K2CO3, KI / acetone; dimethylformamide / Heating 2: 75 percent / AlBr3, NaI / acetonitrile / 0.25 h / 0 °C 3: pyridine / 2 h / 70 - 80 °C 4: KOH / pyridine / 80 °C 5: 90 percent / conc. H2SO4, acetic acid / 1 h / 50 °C 6: 67 percent / dimethyldioxirane / acetone / 0 °C 7: 92 percent / K2CO3 / acetone / Heating 8: 93 percent / AlCl3 / acetonitrile / 0.5 h / Ambient temperature 9: 60 percent / K2CO3 / methanol / 1.5 h / Heating 10: 87 percent / H2 / 10percent Pd/C / methanol; ethyl acetate / Ambient temperature View Scheme
参考文献
Horie, Tokunaru; Shibata, Kenichi; Yamashita, Kazuyo; Kawamura, Yasuhiko; Tsukayama, Masao
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 3 p. 446 - 451
3162-52-5
→
反应条件
74161-28-7
反应条件
1: 83 percent / K2CO3, KI / acetone; dimethylformamide / Heating 2: 75 percent / AlBr3, NaI / acetonitrile / 0.25 h / 0 °C 3: pyridine / 2 h / 70 - 80 °C 4: KOH / pyridine / 80 °C 5: 92 percent / conc. H2SO4, acetic acid / 1 h / 50 °C 6: 74 percent / dimethyldioxirane / acetone / 0 °C 7: 85 percent / K2CO3 / acetone / Heating 8: 83 percent / AlCl3 / acetonitrile / 0.5 h / Ambient temperature 9: 88 percent / K2CO3 / methanol / 1.5 h / Heating 10: 89 percent / H2 / 10percent Pd/C / methanol; ethyl acetate / Ambient temperature View Scheme
参考文献
Horie, Tokunaru; Shibata, Kenichi; Yamashita, Kazuyo; Kawamura, Yasuhiko; Tsukayama, Masao
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 3 p. 446 - 451
3162-52-5
→
反应条件
519-96-0
2-(3,4-二羟基苯基)-3,5,7-三羟基-6-甲氧基-4-苯并吡喃酮
反应条件
1: 83 percent / K2CO3, KI / acetone; dimethylformamide / Heating 2: 75 percent / AlBr3, NaI / acetonitrile / 0.25 h / 0 °C 3: pyridine / 2 h / 70 - 80 °C 4: KOH / pyridine / 80 °C 5: 97 percent / conc. H2SO4, acetic acid / 1 h / 50 °C 6: 70 percent / dimethyldioxirane / acetone / 0 °C 7: 81 percent / K2CO3 / acetone / Heating 8: 97 percent / AlCl3 / acetonitrile / 0.5 h / Ambient temperature 9: 96 percent / K2CO3 / methanol / 1.5 h / Heating 10: 74 percent / H2 / 10percent Pd/C / methanol; ethyl acetate / Ambient temperature View Scheme
参考文献
Horie, Tokunaru; Shibata, Kenichi; Yamashita, Kazuyo; Kawamura, Yasuhiko; Tsukayama, Masao
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 3 p. 446 - 451
