甲基-4,6-O-亚苄基-Α-D-吡喃葡糖苷合成路线 (共 91 条)
反应条件
in acetonitrile Heating;
参考文献
Carbohydrate Research, , vol. 102, p. 147 - 158
反应条件
di-methyltin dichloride; potassium carbonate in tetrahydrofuran T=20°C; Acylation; 12 h;
参考文献
Iwasaki, Fumiaki; Maki, Toshihide; Onomura, Osamu; Nakashima, Waka; Matsumura, Yoshihiro
Journal of Organic Chemistry, 2000 , vol. 65, # 4 p. 996 - 1002
反应条件
N-ethyl-N,N-diisopropylamine in chloroform T=-40°C; 4 h; Reagent/catalystTemperatureSolvent; regioselective reaction;
参考文献
Allen, C. Liana; Miller, Scott J.
Organic Letters, 2013 , vol. 15, # 24 p. 6178 - 6181
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran T=0 - 60°C; Mitsunobu reaction; regioselective reaction;
参考文献
Wang, Guijun; Ella-Menye, Jean-Rene; St. Martin, Michael; Yang, Hao; Williams, Kristopher
Organic Letters, 2008 , vol. 10, # 19 p. 4203 - 4206
反应条件
triethylamine in dichloromethane T=20°C;
参考文献
Lu, Xin-An; Chou, Chien-Hung; Wang, Cheng-Chung; Hung, Shang-Cheng
Synlett, 2003 , # 9 SPEC. ISS. p. 1364 - 1366
反应条件
triethylamine in dichloromethane
参考文献
Battistelli, Chiara Laura; De Castro, Cristina; Iadonisi, Alfonso; Lanzetta, Rosa; Mangoni, Lorenzo; Parrilli, Michelangelo
Journal of Carbohydrate Chemistry, 1999 , vol. 18, # 1 p. 69 - 86
反应条件
1: Me-4,6-(Bz)-α-D-glcp With pyridine in 1,2-dichloro-ethane T=20°C; 1 h; 2: benzoyl chloride in 1,2-dichloro-ethane T=20°C;
参考文献
Bredenkamp, Martin W.; Spies, Hendrik S. C.
Tetrahedron Letters, 2000 , vol. 41, # 4 p. 543 - 546
反应条件
pyridine; benzoic acid anhydride
参考文献
Jeanloz; Jeanloz
Journal of the American Chemical Society, 1957 , vol. 79, p. 2579,2581, 2582
反应条件
N-ethyl-N,N-diisopropylamine; copper dichloride in acetonitrile 4 h; Cooling; Reagent/catalyst; regioselective reaction;
参考文献
Allen, C. Liana; Miller, Scott J.
Organic Letters, 2013 , vol. 15, # 24 p. 6178 - 6181
反应条件
N-ethyl-N,N-diisopropylamine in acetonitrile 4 h; Cooling; Reagent/catalyst; regioselective reaction;
参考文献
Allen, C. Liana; Miller, Scott J.
Organic Letters, 2013 , vol. 15, # 24 p. 6178 - 6181