2-(4-溴苯基)-1,3-苯并噁唑合成路线 (共 35 条)
反应条件
1: pyridine; copper(I) bromide / dichloromethane / 48 h / 20 °C / Molecular sieve 2: hydrazine / methanol; chloroform; water / 12 h / 20 °C 3: acetic acid / water / 0.5 h / 20 °C 4: oxygen; copper(II) bis(trifluoromethanesulfonate) / toluene / 3 h / 80 °C View Scheme
参考文献
Guru, Murali Mohan; Ali, Md Ashif; Punniyamurthy, Tharmalingam
Journal of Organic Chemistry, 2011 , vol. 76, # 13 p. 5295 - 5308
反应条件
1: sodium periodate; sodium acetate; acetic acid / 2 h / Reflux 2: 1,10-phenanthroline; palladium diacetate; caesium carbonate / dimethyl sulfoxide / 20 h / 150 °C / Inert atmosphere View Scheme
参考文献
Yu, Peng; Zhang, Guangyou; Chen, Fan; Cheng, Jiang
Tetrahedron Letters, 2012 , vol. 53, # 34 p. 4588 - 4590
反应条件
palladium dichloride in chlorobenzene 5 h; Reflux; Overall yield = 87 percent;
参考文献
Xie, Hou-Zhi; Gao, Qi; Liang, Ying; Wang, Heng-Shan; Pan, Ying-Ming
Green Chemistry, 2014 , vol. 16, # 4 p. 2132 - 2135
参考文献
Skraup
Justus Liebigs Annalen der Chemie, 1919 , vol. 419, p. 65
反应条件
in methanol Irradiationother solvents; var. quenchers; Quantum yield;
参考文献
Fery-Forgues, Suzanne; Paillous, Nicole
Journal of Organic Chemistry, 1986 , vol. 51, # 5 p. 672 - 677