7-甲氧基-4,9-二氢-3H-吡啶并[3,4-b]吲哚合成路线 (共 6 条)
反应条件
indole; benzeneseleninic anhydride in tetrahydrofuran T=20°C; 48 h;
参考文献
Pouilhes, Annie; Langlois, Yves
Heterocycles, 1985 , vol. 23, # 4 p. 935 - 938
反应条件
trichlorophosphate in acetonitrile T=0°C; 3 h; Inert atmosphere;
参考文献
Lalonde, Mathieu P.; McGowan, Meredeth A.; Rajapaksa, Naomi S.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2013 , vol. 135, # 5 p. 1891 - 1894
反应条件
2: 100 percent / LiAlH4 / tetrahydrofuran 3: 44 percent / benzeneseleninic anhydride, indole / tetrahydrofuran / 48 h / 20 °C View Scheme
参考文献
Pouilhes, Annie; Langlois, Yves
Heterocycles, 1985 , vol. 23, # 4 p. 935 - 938
反应条件
1: 100 percent / LiAlH4 / tetrahydrofuran 2: 44 percent / benzeneseleninic anhydride, indole / tetrahydrofuran / 48 h / 20 °C View Scheme
参考文献
Pouilhes, Annie; Langlois, Yves
Heterocycles, 1985 , vol. 23, # 4 p. 935 - 938
反应条件
2: 100 percent / LiAlH4 / tetrahydrofuran 3: 44 percent / benzeneseleninic anhydride, indole / tetrahydrofuran / 48 h / 20 °C View Scheme
参考文献
Pouilhes, Annie; Langlois, Yves
Heterocycles, 1985 , vol. 23, # 4 p. 935 - 938
反应条件
1: triethylamine / methanol / 16 h / 100 °C / |Inert atmosphere 2: trichlorophosphate / acetonitrile / 3 h / 0 °C / |Inert atmosphere View Scheme
参考文献
Lalonde, Mathieu P.; McGowan, Meredeth A.; Rajapaksa, Naomi S.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2013 , vol. 135, # 5 p. 1891 - 1894