10,10-二氧代噻吨-9-酮合成路线 (共 39 条)
反应条件
1: 56 percent / glacial acetic acid / ethanol / 1 h / Ambient temperature 2: 20 percent / 35percent vol. H2O2 / acetic acid / 48 h / Ambient temperature View Scheme
参考文献
El-Sakka; Zied; Abdel-Bary; Abdel-Mageed
Archiv der Pharmazie, 1994 , vol. 327, # 3 p. 133 - 135
反应条件
sulfuric acid; dihydrogen peroxide; acetic acid Ambient temperature;
参考文献
Taljaard, Benjamin; Goosen, Andre; McCleland, Cedric W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 931 - 934
反应条件
hydrogenchloride; H2O in 1,4-dioxane; water Yield given. Yields of byproduct given;
参考文献
Harwood, John S.; Ternay, Andrew L.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 1657 - 1660
反应条件
in tetrahydrofuran T=22.4°C; Rate constant;
参考文献
Tagaya, Hideyuki; Aruga, Tamotsu; Ito, Osamu; Matsuda, Minoru
Journal of the American Chemical Society, 1981 , vol. 103, # 18 p. 5484 - 5489
反应条件
in tetrahydrofuran T=22.4°C; Rate constant;
参考文献
Tagaya, Hideyuki; Aruga, Tamotsu; Ito, Osamu; Matsuda, Minoru
Journal of the American Chemical Society, 1981 , vol. 103, # 18 p. 5484 - 5489
反应条件
in tetrahydrofuran T=22.4°C; Rate constant;
参考文献
Tagaya, Hideyuki; Aruga, Tamotsu; Ito, Osamu; Matsuda, Minoru
Journal of the American Chemical Society, 1981 , vol. 103, # 18 p. 5484 - 5489
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=22.4°C; Rate constant;
参考文献
Tagaya, Hideyuki; Aruga, Tamotsu; Ito, Osamu; Matsuda, Minoru
Journal of the American Chemical Society, 1981 , vol. 103, # 18 p. 5484 - 5489
反应条件
in tetrahydrofuran T=22.4°C; Rate constant;
参考文献
Tagaya, Hideyuki; Aruga, Tamotsu; Ito, Osamu; Matsuda, Minoru
Journal of the American Chemical Society, 1981 , vol. 103, # 18 p. 5484 - 5489
反应条件
in tetrahydrofuran T=22.4 - 33.5°C; Ea, ΔG*, ΔS*; Rate constantThermodynamic data;
参考文献
Tagaya, Hideyuki; Aruga, Tamotsu; Ito, Osamu; Matsuda, Minoru
Journal of the American Chemical Society, 1981 , vol. 103, # 18 p. 5484 - 5489
反应条件
1: potassium permanganate 2: concentrated sulfuric acid / 125 °C View Scheme
参考文献
Graebe; Schultess
Justus Liebigs Annalen der Chemie, 1891 , vol. 263, p. 14