1-(2-甲基-1-环戊烯基)乙酮合成路线 （共 47 条）
反应条件
aluminum oxide in dichloromethane 12 h; Ambient temperature;
参考文献
Hudlicky, T.; Srnak, T.
Tetrahedron Letters, 1981 , vol. 22, # 35 p. 3351 - 3354
反应条件
1: 52 percent / DBU / toluene / 20 h / Ambient temperature 2: 1) tBuOK, 2) Pd(dppe) / 1) THF, r.t., 10 min, 2) THF, 20 deg C, 3 h View Scheme
参考文献
Monteiro, Nuno; Gore, Jacques; Balme, Genevieve
Tetrahedron, 1992 , vol. 48, # 46 p. 10103 - 10114
反应条件
1: 52 percent / pyridinium dichromate / dimethylformamide / 6 h / Ambient temperature 2: 87 percent / Al2O3 (Woelm neutral for TLC) / 48 h / Ambient temperature View Scheme
参考文献
Zaidlewicz, Marek
Synthesis, 1988 , # 9 p. 701 - 703
反应条件
1: 2.) 3 M aq. NaOH / 1.) ether, room temp., 3 h, 2.) room temp., 6 h 2: 52 percent / pyridinium dichromate / dimethylformamide / 6 h / Ambient temperature 3: 87 percent / Al2O3 (Woelm neutral for TLC) / 48 h / Ambient temperature View Scheme
参考文献
Zaidlewicz, Marek
Synthesis, 1988 , # 9 p. 701 - 703
反应条件
1: 87 percent / diethyl ether / 1 h 2: 1.) zinc chloride, 2.) sodium methoxide / 1.) 0 deg C, 2 h, 2.) MeOH, r.t., 8 h View Scheme
参考文献
Hudlicky, Tomas; Kwart, Lawrence D.; Tiedje, Mark H.; Ranu, Brindaban C.; Short, Robert P.; et al.
Synthesis, 1986 , # 9 p. 716 - 727
反应条件
1: 70 percent / 10percent HBF4, HgO / tetrahydrofuran / Ambient temperature 3: tetrahydrofuran / -78 °C View Scheme
参考文献
Dieter, R. Karl; Jenkitkasemwong, Yawares
Tetrahedron Letters, 1982 , vol. 23, # 37 p. 3747 - 3750
反应条件
in tetrahydrofuran T=-78°C;
参考文献
Dieter, R. Karl; Jenkitkasemwong, Yawares
Tetrahedron Letters, 1982 , vol. 23, # 37 p. 3747 - 3750
反应条件
zinc(II) chloride T=0°C; 2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Hudlicky, Tomas; Kwart, Lawrence D.; Tiedje, Mark H.; Ranu, Brindaban C.; Short, Robert P.; et al.
Synthesis, 1986 , # 9 p. 716 - 727
反应条件
potassium hydroxide in ethanol Heating;
参考文献
Kossanyi,J.
Bulletin de la Societe Chimique de France, 1965 , p. 722 - 732
参考文献
Brown,F. et al.
Tetrahedron Letters, 1966 , p. 6115 - 6119
