3-硝基-4-甲氧基苯甲醛合成路线 (共 45 条)
反应条件
Mg(NO3)2*6H2O; AMA T=20°C; 0.5 h; Neat (no solvent);
参考文献
Hosseini-Sarvari, Mona; Tavakolian, Mina
Journal of Chemical Research, 2008 , # 12 p. 722 - 724
反应条件
Bi(NO3)3·5H2O in 1,2-dichloro-ethane T=80 - 85°C; 40 h; Overall yield = 85 percentChromat.;
参考文献
Tetrahedron Letters, , vol. 53, # 50 p. 6782 - 6785,4
参考文献
Synthesis, , # 3 p. 405 - 410
反应条件
lead(IV) acetate in benzene Heating;
参考文献
Shankaran, K.; Rao, A.S.
Synthetic Communications, 1980 , vol. 10, # 7 p. 573 - 580
反应条件
trifluoromethylsulfonic anhydride; [EtNH3][NO3] T=0 - 20°C; 0.666667 h; Inert atmosphere;
参考文献
Aridoss, Gopalakrishnan; Laali, Kenneth K.
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 8088 - 8094
反应条件
1: thionyl chloride; N,N-dimethyl-formamide / toluene / 20 °C 2: triethylamine / dichloromethane / 0 - 20 °C 3: zirconocene dichloride; lithium tri-t-butoxyaluminum hydride / tetrahydrofuran / 0.33 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 16, # 2 p. 390 - 393
反应条件
1: triethylamine / dichloromethane / 0 - 20 °C 2: zirconocene dichloride; lithium tri-t-butoxyaluminum hydride / tetrahydrofuran / 0.33 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 16, # 2 p. 390 - 393
反应条件
ammonium cerium(IV) nitrate; trifluoroacetic acid T=23°C; 1 h; dinitrogen tetroxide in CH3CN, 1 h;
参考文献
Canadian Journal of Chemistry, , vol. 66, p. 1670 - 1674
反应条件
1: polyphosphoric acid 2: 96 percent / sodium borohydride / ethanol 3: 66 percent / lead tetraacetate / benzene / Heating View Scheme
参考文献
Synthetic Communications, , vol. 10, # 7 p. 573 - 580
反应条件
in methanol Substitution; 24 h; Heating;
参考文献
Tetrahedron, , vol. 56, # 3 p. 447 - 453