3-硝基-4-甲氧基苯甲醛合成路线 （共 45 条）
参考文献
Justus Liebigs Annalen der Chemie, , vol. 243, p. 370
反应条件
in ethanol T=20°C; 240 h; Product distribution;
参考文献
Blokhin, A.V.; Bundel, Yu. G.; Terenin, V.I.; Kurtz, A.L.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 11 p. 2116 - 2123
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 11 p. 2399 - 2406
反应条件
ammonium chloride; nickel in water 2 h; Heating;
参考文献
Han, Xiaojun; Pradeep, Singh N. D.; Critchley, Kevin; Sheikh, Khizar; Bushby, Richard J.; Evans, Stephen D.
Chemistry - A European Journal, 2007 , vol. 13, # 28 p. 7957 - 7964
反应条件
in ethanol T=20°C; 240 h; Product distribution;
参考文献
Blokhin, A.V.; Bundel, Yu. G.; Terenin, V.I.; Kurtz, A.L.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 11 p. 2116 - 2123
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 11 p. 2399 - 2406
反应条件
1: With sodium tetrahydroborate in tetrahydrofuran; ethanol T=10 - 20°C; 2.16667 h; 2: With water T=20°C; 0.5 h;
参考文献
AVENTIS PHARMA SA
Patent: JP2005/522478 A, 2005 ;
Location in patent: Page/Page column 9 ;
反应条件
1: sodium tetrahydroborate / methanol / 1 h / 0 - 5 °C / Inert atmosphere 2: phosphorus tribromide / toluene / 0.5 h / 40 - 100 °C / Inert atmosphere 3: sodium hydroxide / methanol / 3 h / 20 °C / Inert atmosphere View Scheme
参考文献
Reddy, M. V. Ramana; Venkatapuram, Padmavathi; Mallireddigari, Muralidhar R.; Pallela, Venkat R.; Cosenza, Stephen C.; Robell, Kimberly A.; Akula, Balaiah; Hoffman, Benjamin S.; Reddy, E. Premkumar
Journal of Medicinal Chemistry, 2011 , vol. 54, # 18 p. 6254 - 6276
反应条件
potassium permanganate
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 45, p. 45
反应条件
1: potassium permanganate 2: HNO3+H2SO4 View Scheme
参考文献
de Lange
Recueil des Travaux Chimiques des Pays-Bas, 1926 , vol. 45, p. 45
反应条件
1: sodium tetrahydroborate / methanol / 1 h / 0 - 5 °C / Inert atmosphere 2: phosphorus tribromide / toluene / 0.5 h / 40 - 100 °C / Inert atmosphere 3: sodium hydroxide / methanol / 3 h / 20 °C / Inert atmosphere 4: dihydrogen peroxide; acetic acid / water / 24 h / 20 °C / Inert atmosphere View Scheme
参考文献
Reddy, M. V. Ramana; Venkatapuram, Padmavathi; Mallireddigari, Muralidhar R.; Pallela, Venkat R.; Cosenza, Stephen C.; Robell, Kimberly A.; Akula, Balaiah; Hoffman, Benjamin S.; Reddy, E. Premkumar
Journal of Medicinal Chemistry, 2011 , vol. 54, # 18 p. 6254 - 6276
反应条件
hydrogenchloride in ethanol; dichloromethane
