pyridine in dichloromethane T=0 - 20°C; Inert atmosphere;
参考文献
Hicks, Jacqueline D.; Hyde, Alan M.; Cuezva, Alberto Martinez; Buchwald, Stephen L.
Journal of the American Chemical Society, 2009 , vol. 131, # 46 p. 16720 - 16734
1: With [{(η5-C5Me5)IrCl}2(μ-Cl)2]; [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2 in neat (no solvent) T=130°C; 3 h; Inert atmosphereSchlenk techniqueGreen chemistry; 2: With caesium carbonate in neat (no solvent) T=150°C; 12 h; Inert atmosphereSchlenk techniqueGreen chemistry;
