3-(4-氟苯基)-5(4H)-异噁唑酮合成路线 (共 5 条)
反应条件
sodium hydrogencarbonate; ammonium chloride in ethanol 4 h; Reflux;
参考文献
Bayer CropScience AG
Patent: US2012/65063 A1, 2012 ;
Location in patent: Page/Page column 22 ;
反应条件
pyridine; hydroxylamine hydrochloride in ethanol Reflux;
参考文献
Kafle, Bhooshan; Aher, Nilkanth G.; Khadka, Deegendra; Park, Hwangseo; Cho, Hyeongjin
Chemistry - An Asian Journal, 2011 , vol. 6, # 8 p. 2073 - 2079
反应条件
1: manganese(IV) oxide / dichloromethane / 20 °C 2: pyridine; hydroxylamine hydrochloride / ethanol / Reflux View Scheme
参考文献
Kafle, Bhooshan; Aher, Nilkanth G.; Khadka, Deegendra; Park, Hwangseo; Cho, Hyeongjin
Chemistry - An Asian Journal, 2011 , vol. 6, # 8 p. 2073 - 2079
反应条件
1: ammonium chloride; zinc 2: manganese(IV) oxide / dichloromethane / 20 °C 3: pyridine; hydroxylamine hydrochloride / ethanol / Reflux View Scheme
参考文献
Kafle, Bhooshan; Aher, Nilkanth G.; Khadka, Deegendra; Park, Hwangseo; Cho, Hyeongjin
Chemistry - An Asian Journal, 2011 , vol. 6, # 8 p. 2073 - 2079
反应条件
(i) nBuLi, THF, (ii) /BRN= 1900390/, aq. HCl; Multistep reaction;
参考文献
Griffiths,J.S. et al.
Journal of the Chemical Society [Section] C: Organic, 1971 , p. 974 - 975