4,5-二甲基-1,2-苯二胺合成路线 （共 140 条）
反应条件
in N,N-dimethyl-formamide
Heating;
参考文献
Merchan; Garin; Melendez; Tejero
Synthesis, 1982 , vol. No. 12, p. 1066 - 1067
反应条件
in N,N-dimethyl-formamide
Heating;
参考文献
Merchan; Garin; Melendez; Tejero
Synthesis, 1982 , vol. No. 12, p. 1066 - 1067
反应条件
1: 61 percent / Et3N; NaI / tetrahydrofuran / 60 °C
2: 59 percent / boron oxide; acetic acid / 3 h / 60 °C
3: 91 percent / K2CO3 / dimethylformamide / 60 °C
View Scheme
参考文献
Carroll, Joseph B.; Jordan, Brian J.; Xu, Hao; Erdogan, Belma; Lee, Lisa; Cheng, Lily; Tiernan, Christopher; Cooke, Graeme; Rotello, Vincent M.
Organic Letters, 2005 , vol. 7, # 13 p. 2551 - 2554
反应条件
2: chromium(VI) oxide; acetic acid / water / 0.08 h / 90 - 100 °C
View Scheme
参考文献
Ge, Yan Qing; Jia, Jiong; Yang, He; Tao, Xu Tang; Wang, Jian Wu
Dyes and Pigments, 2011 , vol. 88, # 3 p. 344 - 349
反应条件
tin(ll) chloride in neat (no solvent)
T=170°C; 5 h;
参考文献
Chen, Ren-Hong; Xiong, Jin-Feng; Peng, Pai; Mo, Guang-Zhen; Tang, Xing-San; Wang, Zhao-Yang; Wang, Xiu-Fang
Asian Journal of Chemistry, 2014 , vol. 26, # 3 art. no. 16438, p. 926 - 932
反应条件
2: water; HCl
View Scheme
参考文献
Mamalis et al.
Journal of the Chemical Society, 1950 , p. 1600,1602
反应条件
in water; acetic acid
10 h; Heating;
参考文献
Sallam, Mohammed A. E.; Abdel Megid, Somia M. E.
Carbohydrate Research, 1984 , vol. 125, p. 85 - 96
反应条件
hydrogenchloride; water
参考文献
King; Felton
Journal of the Chemical Society, 1948 , p. 1371
反应条件
aminosulfonic acid in methanol
T=20°C; 0.7 h;
参考文献
Zhang, Zhan-Hui; Li, Tong-Shuang; Li, Jian-Jiong
Monatshefte fur Chemie, 2007 , vol. 138, # 1 p. 89 - 94
反应条件
in ethanol; acetic acid
12 h; Heating;
参考文献
Helissey, Philippe; Desbene-Finck, Stephanie; Giorgi-Renault, Sylviane
European Journal of Organic Chemistry, 2005 , # 2 p. 410 - 415
