4,5-二甲基-1,2-苯二胺合成路线 （共 140 条）
反应条件
in xylene
T=136°C; 0.166667 h; Irradiation;
参考文献
Bougrin, Khalid; Bennani, A. Kella; Tetouani, Souad Fkih; Soufiaoui, Mohamed
Tetrahedron Letters, 1994 , vol. 35, # 45 p. 8373 - 8376
反应条件
in xylene
4.5 h; Heating;
参考文献
Meth-Cohn, Otto; Smith, David I.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 261 - 270
反应条件
in acetonitrile
T=20°C;
参考文献
Shaabani, Ahmad; Maleki, Ali; Hajishaabanha, Fatemeh; Mofakham, Hamid; Seyyedhamzeh, Mozhdeh; Manyari, Mojtaba; Ng, Seik Weng
Journal of Combinatorial Chemistry, 2010 , vol. 12, # 1 p. 186 - 190
反应条件
(E,Z)-crotononitrile; 10 Pd/C; acetic acid in water; toluene
T=170°C; P=15514.9 Torr; 1.5 h; Microwave irradiationInert atmosphere;
参考文献
Pizzetti, Marianna; De Luca, Elisa; Petricci, Elena; Taddei, Maurizio; Porcheddu, Andrea
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 13 p. 2453 - 2464,12
Title/Abstract Full Text Show Details
Pizzetti, Marianna; De Luca, Elisa; Petricci, Elena; Porcheddu, Andrea; Taddei, Maurizio
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 13 p. 2453 - 2464
反应条件
activated alumina balls calcined at 700 °C in neat (no solvent)
T=150°C; 5 h; Green chemistry;
参考文献
Ghosh, Sabari; Hudrlik, Anne; Mukhopadhyay, Chhanda
Journal of the Indian Chemical Society, 2013 , vol. 90, # 10 p. 1737 - 1748
反应条件
1: 31 percent / 1.) polyphosphoric acid; 2.) Na2CO3; 3.) 50percent aq. HBF4 / 1.) 165-170 deg C, 12 h; 2.) pH=8; 3.) pH=5
2: 68 percent / acetonitrile / 40 h / 100 °C
View Scheme
参考文献
Alcalde, Ermitas; Gisbert, Maria; Perez-Garcia, Lluisa
Chemistry Letters, 1992 , # 12 p. 2357 - 2360
反应条件
HOF* CH3CN; NAF in dichloromethane; water; acetonitrile
T=-15°C; 0.0666667 h;
参考文献
Golan, Elizabeth; Rozen, Shlomo
Journal of Organic Chemistry, 2003 , vol. 68, # 23 p. 9170 - 9172
反应条件
pyridine in tetrahydrofuran
T=20°C; 2 h;
参考文献
Kurbatov; Kuznetsov; Simakov; Voronina; Zhdanov; Olekhnovich
Russian Journal of General Chemistry, 2004 , vol. 74, # 5 p. 731 - 737
参考文献
Kaupp, Gerd; Naimi-Jamal, M. Reza; Schmeyers, Jens
Chemistry - A European Journal, 2002 , vol. 8, # 3 p. 594 - 600
反应条件
in ethanol
0.166667 h;
参考文献
Moemeni, Mehdi; Arvinnezhad, Hamid; Samadi, Saadi; Tajbakhsh, Mahmood; Jadidi, Khosrow; Khavasi, Hamid Reza
Journal of Heterocyclic Chemistry, 2012 , vol. 49, # 1 p. 190 - 194
