in neat (no solvent)
photodetachging after NCO formation from BzNCO in a TOF mass-spectrometer;
参考文献
Hoops; Hoops, Alexandra A.; Bise; Bise, Ryan T.; Gascooke; Gascooke, Jason R.; Neumark; Neumark, Daniel M.
Journal of Chemical Physics, 2001 , vol. 114, # 20 p. 9020 - 9027
other Radiation; benzyl isocyanate is dropped in He or in mixture of He and 40percent CF4 at 3 atm pressure, the material is expanded through a pulsed molecular beam valve and irradiated by perpendicular electron beam;
参考文献
Bradforth, Stephen E.; Kim, Eun Ha; Arnold, Don W.; Neumark, Daniel M.
Journal of Chemical Physics, 1993 , vol. 98, # 2 p. 800 - 810
1: 65 percent / sulfuryl chloride, azobisisobutyronitrile / 7 h / 70 - 90 °C
2: 42 percent / 75 - 110 °C
View Scheme
参考文献
Kozhushko, B. N.; Gumenyuk, A. V.; Mikhailyuchenko, N. K.; Shokol, V. A.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 3 p. 541 - 549,430 - 437