2-丁基-1,3-二氢-1,3,2-苯并二氮杂硼杂环戊二烯合成路线 （共 7 条）
反应条件
in xylene byproducts: H2O; distilling the water with the solvent; filtering, recrystn. from benzene or CCl4;
参考文献
Matteson,D.S.; Waldbillig,J.O.
Journal of Organic Chemistry, 1963 , vol. 28, p. 366 - 369
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Nyilas; Soloway
Journal of the American Chemical Society, 1959 , vol. 81, p. 2681
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Letsinger, R. L.; Hamilton, S. B.
Journal of the American Chemical Society, 1958 , vol. 80, p. 5411 - 5413
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Gmelin Handbook: B: B-Verb.1, 2.8.2.1.3, page 168 - 175
反应条件
BuMgX in tetrahydrofuran
参考文献
Gmelin Handbook: B: B-Verb.1, 2.8.2.1.3, page 168 - 175
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Hohnstedt, L. F.; Pellicciotto, A. M.
U.S. Dept. Comm. Office Tech. Serv. AD 230544 (1959)
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Pellicciotto, A. M.
Diss. St. Louis Univ. 1962.
反应条件
in benzene byproducts: H2; reflux, then cooling and adding pentane to the mixture; recrystn. from benzene-pentane;
参考文献
Hawthorne,M.F.
Journal of the American Chemical Society, 1961 , vol. 83, p. 831 - 833
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Hawthorne
Journal of the American Chemical Society, 1959 , vol. 81, p. 5836
Journal of the American Chemical Society, 1961 , vol. 83, p. 831
Full Text View citing articles Show Details
Gmelin Handbook: B: B-Verb.1, 2.8.2.1.3, page 168 - 175
参考文献
Hawthorne,M.F.
Journal of the American Chemical Society, 1961 , vol. 83, p. 831 - 833
反应条件
3: water / diethyl ether View Scheme
参考文献
Pellicciotto, A. M.
Diss. St. Louis Univ. 1962
反应条件
1: chlorobenzene 2: water / diethyl ether View Scheme
参考文献
Pellicciotto, A. M.
Diss. St. Louis Univ. 1962
参考文献
Gerrard,W. et al.
Journal of the Chemical Society, 1964 , p. 740 - 745
