4-羟基-β-硝基苯乙烯合成路线 (共 14 条)
反应条件
AP-E1 T=90°C; Henry Reaction; 0.25 - 0.266667 h; Product distribution / selectivity;
参考文献
SYRACUSE UNIVERSITY
Patent: US2009/43134 A1, 2009 ;
Location in patent: Page/Page column 24 ;
反应条件
tert.-butylnitrite; silica gel in acetonitrile T=100°C; P=2250.23 Torr; Microwave irradiation; TimeTemperaturePressure;
参考文献
Kumar, M. Satish; Rajanna; Reddy, K. Rajendar; Venkateswarlu; Venkanna
Synthetic Communications, 2013 , vol. 43, # 19 p. 2672 - 2677
反应条件
APUD1 T=90°C; Henry Reaction; Product distribution / selectivity;
参考文献
US2009/43134 A1, ;
Page/Page column 15; 16 ;
反应条件
APUD1 T=90°C; Henry Reaction; 0.25 - 1 h; Product distribution / selectivity;
参考文献
US2009/43134 A1, ;
Page/Page column 4; 15; 16; Sheet 66/106 ;
反应条件
primary amine-functionalized mesoporous silica catalyst T=90°C; P=760.051 Torr; Continuous flow fixed bed glass reactor;
参考文献
Applied Catalysis A: General, , vol. 389, # 1-2 p. 19 - 26
反应条件
mesoporous silica nanoparticles-NNH2-SO3H T=90°C; nitroaldol Henry reaction; 6 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 15, # 29 p. 7052 - 7062
反应条件
mesoporous silica nanoparticles-NNH2-SO3H T=90°C; nitroaldol Henry reaction; 6 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 15, # 29 p. 7052 - 7062
参考文献
Journal of the Chemical Society, , vol. 99, p. 286
反应条件
1: aqueous-alcoholic KOH-solution / 0 °C 2: diluted alcoholic hydrochloric acid View Scheme
参考文献
Journal of the Chemical Society, , vol. 99, p. 286
参考文献
Rosenmund; Pfannkuch
Chemische Berichte, 1922 , vol. 55, p. 2365