1-(4-甲氧苯基)-2-硝基乙烯合成路线 (共 57 条)
反应条件
titanium tetrachloride; tetraethylammonium p-toluenesulfonate in N,N-dimethyl-formamide electroreduction - 4 mA/cm2;
参考文献
Synthesis, , # 7 p. 631 - 633
反应条件
in benzene 8 h; Heating;
参考文献
Rao; Ravishankar; Trivedi
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 3 p. 207 - 214
反应条件
acetic acid in N,N-dimethyl-formamide T=150°C; 0.333333 h; Microwave irradiation; chemoselective reaction;
参考文献
Che, Jun; Lam, Yulin
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 10 p. 1752 - 1758
参考文献
G.D. Searle and Co.
Patent: US6011028 A1, 2000 ;
参考文献
G. D. Searle and Co.
Patent: US5883251 A1, 1999 ;
参考文献
Itoh, Kazuyoshi; Ishida, Hideaki; Chikashita, Hidenori
Chemistry Letters, 1982 , p. 1117 - 1118
反应条件
tri-n-butyl-tin hydride; ozone 1.) methylene chloride; Multistep reaction;
参考文献
Aizpurua, J. M.; Oiarbide, M.; Palomo, C.
Tetrahedron Letters, 1987 , vol. 28, # 44 p. 5365 - 5366
反应条件
1: 4-OCH3 β-NO2 styrene With (S)-10,10'-bis[(S)-4-isopropyl-4,5-dihydrooxazol-2-yl]-9,9'-biphenanthrene; zinc(II) trifluoroacetate in diethyl ether T=20°C; 0.25 h; Inert atmosphere; 2: indole in diethyl ether T=20°C; Friedel-Crafts alkylation; Inert atmosphere;
参考文献
Lin, Shuang-zheng; You, Tian-pa
Tetrahedron, 2009 , vol. 65, # 5 p. 1010 - 1016
反应条件
samarium (III) iodide; silica gel Michael reaction; 0.0333333 h; microwave irradiation;
参考文献
Zhan, Zhuang-Ping; Lang, Kai
Synlett, 2005 , # 10 art. no. U09905ST, p. 1551 - 1554
反应条件
anhydrous iron chloride in N,N-dimethyl-formamide T=80°C; Michael Addition; 2 h;
参考文献
Santra, Sougata; Bagdi, Avik Kumar; Majee, Adinath; Hajra, Alakananda
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 6 p. 1065 - 1070