N-[3-(二甲氨基)丙基]月桂酰胺合成路线 (共 8 条)
反应条件
triethylamine in dichloromethane T=20°C;
参考文献
ISAGRO RICERCA S.r.l
Patent: US2009/105238 A1, 2009 ;
Location in patent: Page/Page column 7 ;
参考文献
Limanov, V. E.; Epshtein, A. E.; Yakushkin, M. I.; Telegin, M. Yu.; Kotov, V. I.; et al.
Pharmaceutical Chemistry Journal, 1981 , vol. 15, # 2 p. 85 - 87
Khimiko-Farmatsevticheskii Zhurnal, 1981 , vol. 15, # 2 p. 28 - 30
反应条件
in toluene Inert atmosphereDarkness;
参考文献
Ghumare, Anant K.; Pawar, Balu V.; Bhagwat, Sunil S.
Journal of Surfactants and Detergents, 2013 , vol. 16, # 1 p. 85 - 93
反应条件
T=160 - 200°C; 9 - 11.8 h; Product distribution / selectivity;
参考文献
US2007/10680 A1, ;
Page/Page column 10-12 ;
反应条件
T=120 - 130°C; 24 h;
参考文献
Journal of Fluorine Chemistry, , vol. 131, # 6 p. 704 - 708
反应条件
in diethyl ether T=20°C; 24 h;
参考文献
Ngo, Thi Huong Viet; Damas, Christine; Naejus, Regine; Coudert, Robert
Journal of Fluorine Chemistry, 2010 , vol. 131, # 6 p. 704 - 708
反应条件
in isopropyl alcohol
8 h; Heating;
参考文献
Limanov, V. E.; Epshtein, A. E.; Yakushkin, M. I.; Telegin, M. Yu.; Kotov, V. I.; et al.
Pharmaceutical Chemistry Journal, 1981 , vol. 15, # 2 p. 85 - 87
Khimiko-Farmatsevticheskii Zhurnal, 1981 , vol. 15, # 2 p. 28 - 30
反应条件
in ethyl acetate
T=80°C;
参考文献
Chu, Zonglin; Feng, Yujun
Langmuir, 2012 , vol. 28, # 2 p. 1175 - 1181