1,2-o-异亚丙基-3-o-苯甲酰基-d-异呋喃糖合成路线 （共 10 条）
反应条件
acetic acid T=50°C; 1 h;
参考文献
Alais; David
Carbohydrate Research, 1992 , vol. 230, # 1 p. 79 - 87
反应条件
1: 90 percent / pyridine / 20 h / 20 °C 2: 91 percent / aq, AcOH / 0.75 h / 60 °C View Scheme
参考文献
Kralikova, Sarka; Budesinsky, Milos; Tomeckova, Ivana; Rosenberg, Ivan
Tetrahedron, 2006 , vol. 62, # 41 p. 9742 - 9750
反应条件
1: pyridine / CH2Cl2 / 1 h / 0 °C 2: aq. AcOH / 24 h / 20 °C View Scheme
参考文献
Zheng, Xiaoping; Nair, Vasu
Nucleosides and Nucleotides, 1999 , vol. 18, # 9 p. 1961 - 1976
反应条件
1: 8.0 g / NaBH4 / ethanol / 0.5 h / 0 °C 2: 90 percent / pyridine / 20 h / 20 °C 3: 91 percent / aq, AcOH / 0.75 h / 60 °C View Scheme
参考文献
Nicolaou; Pavia; Seitz
Journal of the American Chemical Society, 1982 , vol. 104, # 7 p. 2027 - 2029
反应条件
1: DMAP / CH2Cl2; pyridine / 1 h / Ambient temperature 2: AcOH, HCOOH / H2O / 1 h / Ambient temperature View Scheme
参考文献
Nicolaou; Pavia; Seitz
Journal of the American Chemical Society, 1982 , vol. 104, # 7 p. 2027 - 2029
反应条件
1: Ru2O, NaIO4 2: NaBH4 3: pyridine 4: aq. H2SO4 View Scheme
参考文献
Pitsch, Stefan
Helvetica Chimica Acta, 1997 , vol. 80, # 8 p. 2286 - 2314
反应条件
1: Et3N / acetonitrile / 15 h / 20 °C 2: aq. AcOH / 3 h / 50 °C View Scheme
参考文献
Kralikova, Sarka; Budesinsky, Milos; Tomeckova, Ivana; Rosenberg, Ivan
Tetrahedron, 2006 , vol. 62, # 41 p. 9742 - 9750
反应条件
1: 68 percent / toluene / 2 h / 100 °C 2: 93 percent / aq. 60percent CH3COOH / 1 h / 50 °C View Scheme
参考文献
Alais; David
Carbohydrate Research, 1992 , vol. 230, # 1 p. 79 - 87
反应条件
1: 68 percent / toluene / 2 h / 100 °C 2: 93 percent / aq. 60percent CH3COOH / 1 h / 50 °C View Scheme
参考文献
Alais; David
Carbohydrate Research, 1992 , vol. 230, # 1 p. 79 - 87
反应条件
1: 91 percent / ZnCl2, H3PO4 / 30 h / Ambient temperature 2: pyridinium dichromate, Ac2O / CH2Cl2 / 2 h / 50 °C 3: NaBH4 / ethanol; H2O / 3 h / Ambient temperature 4: DMAP / CH2Cl2; pyridine / 1 h / Ambient temperature 5: AcOH, HCOOH / H2O / 1 h / Ambient temperature View Scheme
参考文献
Pitsch, Stefan
Helvetica Chimica Acta, 1997 , vol. 80, # 8 p. 2286 - 2314
