3-异丙基-4-甲氧基苯甲醛合成路线 （共 12 条）
反应条件
trichlorophosphate in N-methyl-acetamide; water; ethyl acetate
参考文献
Chidambaram, Ramakrishnan; Kant, Joydeep; Weaver, Raymond E.; Yu, Jurong; Ghosh, Arun
Patent: US2003/157671 A1, 2003 ;
US 20030157671 A1
反应条件
tin(IV) chloride in dichloromethane T=0°C; 1 h;
参考文献
Katoh, Takahiro; Akagi, Taichi; Noguchi, Chie; Kajimoto, Tetsuya; Node, Manabu; Tanaka, Reiko; Nishizawa (nee Iwamoto), Manabu; Ohtsu, Hironori; Suzuki, Noriyuki; Saito, Koichi
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 7 p. 2736 - 2748
反应条件
trichlorophosphate T=80 - 90°C; 16 h; Under N2;
参考文献
WO2004/67482 A2, ;
Page 50-51 ;
WO 2004/067482 A2
反应条件
magnesium in tetrahydrofuran
参考文献
Burnell; Caron
Synthetic Communications, 1991 , vol. 21, # 1 p. 127 - 132
反应条件
1: 78 percent / AlCl3 / CH2Cl2 / 8 h / Ambient temperature 2: 85 percent / diethyl ether / 5 °C 3: 100 percent / 2 h / Heating 4: 99 percent / H2 / Pd/C / diethyl ether / 2068.6 Torr 5: 75 percent / PCC, HOAc, Celite, molecular sieve 4A / CH2Cl2 7: 84 percent / KBr, m-CPBA, 18-cr-6 / CH2Cl2 / 0.5 h / 0 °C 8: 98 percent / Mg / tetrahydrofuran View Scheme
参考文献
Synthetic Communications, , vol. 21, # 1 p. 127 - 132
反应条件
1: 100 percent / 2 h / Heating 2: 99 percent / H2 / Pd/C / diethyl ether / 2068.6 Torr 3: 75 percent / PCC, HOAc, Celite, molecular sieve 4A / CH2Cl2 5: 84 percent / KBr, m-CPBA, 18-cr-6 / CH2Cl2 / 0.5 h / 0 °C 6: 98 percent / Mg / tetrahydrofuran View Scheme
参考文献
Synthetic Communications, , vol. 21, # 1 p. 127 - 132
反应条件
1: 99 percent / H2 / Pd/C / diethyl ether / 2068.6 Torr 2: 75 percent / PCC, HOAc, Celite, molecular sieve 4A / CH2Cl2 4: 84 percent / KBr, m-CPBA, 18-cr-6 / CH2Cl2 / 0.5 h / 0 °C 5: 98 percent / Mg / tetrahydrofuran View Scheme
参考文献
Synthetic Communications, , vol. 21, # 1 p. 127 - 132
反应条件
1: 85 percent / diethyl ether / 5 °C 2: 100 percent / 2 h / Heating 3: 99 percent / H2 / Pd/C / diethyl ether / 2068.6 Torr 4: 75 percent / PCC, HOAc, Celite, molecular sieve 4A / CH2Cl2 6: 84 percent / KBr, m-CPBA, 18-cr-6 / CH2Cl2 / 0.5 h / 0 °C 7: 98 percent / Mg / tetrahydrofuran View Scheme
参考文献
Synthetic Communications, , vol. 21, # 1 p. 127 - 132
反应条件
carbon disulfide; aluminium trichloride
参考文献
Journal of the American Chemical Society, , vol. 57, p. 909,911
反应条件
1: 75 percent / PCC, HOAc, Celite, molecular sieve 4A / CH2Cl2 3: 84 percent / KBr, m-CPBA, 18-cr-6 / CH2Cl2 / 0.5 h / 0 °C 4: 98 percent / Mg / tetrahydrofuran View Scheme
参考文献
Synthetic Communications, , vol. 21, # 1 p. 127 - 132
