4-邻苯二甲酰亚氨基丁腈合成路线 (共 20 条)
参考文献
King; L'Ecuyer; Openshaw
Journal of the Chemical Society, 1936 , p. 352
参考文献
Gabriel
Chemische Berichte, 1889 , vol. 22, p. 3337
Chemische Berichte, 1890 , vol. 23, p. 1772
反应条件
1: diethyl ether; ammonia 2: thionyl chloride View Scheme
参考文献
King; L'Ecuyer; Openshaw
Journal of the Chemical Society, 1936 , p. 352
参考文献
Gabriel
Chemische Berichte, 1889 , vol. 22, p. 3337
Chemische Berichte, 1890 , vol. 23, p. 1772
反应条件
hydrogenchloride; diethyl ether; tin(ll) chloride und Behandeln des Reaktionsprodukts mit Wasser und Aether;
参考文献
King; L'Ecuyer; Openshaw
Journal of the Chemical Society, 1936 , p. 352
反应条件
1: With hydrazine hydrate in ethanol; water T=20°C; 0.25 h; 2: With hydrogenchloride in ethanol; water 3 h; Heating;
参考文献
Ryder; Schweiger; Glidle; Cooper
Journal of Materials Chemistry, 2000 , vol. 10, # 8 p. 1785 - 1793
反应条件
und Destillation des Reaktionsprodukts mit Alkali;
参考文献
Keil
Chemische Berichte, 1926 , vol. 59, p. 2817
参考文献
Gabriel
Chemische Berichte, 1889 , vol. 22, p. 3337
Chemische Berichte, 1890 , vol. 23, p. 1772
反应条件
1: 54.5 percent / H2, HCl conc. / PtO2 / ethanol / 24 h / 2327.2 Torr
2: 87.6 percent / Et3N / CH2Cl2 / 4 h
3: 96 percent / NaNO2 / acetic acid; acetic anhydride / 4 °C
4: 54 percent / Na2CO3 / CCl4 / 40 h / Heating
5: 90.4 percent / NaI / acetone / 2 h / Heating
View Scheme
参考文献
Thiruvengadam; Gould; Aberhart; Horng Jau Lin
Journal of the American Chemical Society, 1983 , vol. 105, # 16 p. 5470 - 5476
参考文献
Gabriel
Chemische Berichte, 1889 , vol. 22, p. 3337
Chemische Berichte, 1890 , vol. 23, p. 1772