2-[1-(2-羟基乙基)环己基]乙醇合成路线 （共 6 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=0 - 20°C;
参考文献
Werz, Daniel B.; Fischer, Felix R.; Kornmayer, Stefan C.; Rominger, Frank; Gleiter, Rolf
Journal of Organic Chemistry, 2008 , vol. 73, # 20 p. 8021 - 8029
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=0°C; 3 h;
参考文献
ONO PHARMACEUTICAL CO., LTD.
Patent: EP1889622 A1, 2008 ;
Location in patent: Page/Page column 40 ;
EP 1889622 A1
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Freed,M.E.; Rice,L.M.
Journal of Heterocyclic Chemistry, 1965 , vol. 2, p. 214 - 217
反应条件
1: aq. H2SO4 2: aq. H2SO4 3: LiAlH4 / diethyl ether View Scheme
参考文献
Handley,G.J. et al.
Australian Journal of Chemistry, 1960 , vol. 13, p. 129 - 144
反应条件
hydrogen bromide in sulfuric acid 20 h; Heating;
参考文献
Eilbracht, Peter; Acker, Michael; Totzauer, Walter
Chemische Berichte, 1983 , vol. 116, # 1 p. 238 - 242
反应条件
sulfuric acid; hydrogen bromide
参考文献
Ashley et al.
Journal of the Chemical Society, 1958 , p. 3298,3308
