2,4-二羟基-6-甲基苯甲酸甲酯合成路线 (共 72 条)
参考文献
Asahina; Akagi
Chemische Berichte, 1935 , vol. 68, p. 1130,1132
Yakugaku Zasshi, 1935 , vol. 55, p. 1117,1121
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Nolan; Keane; Davidson
Scientific Proceedings of the Royal Dublin Society, 1940 , vol. 22, p. 237
反应条件
bromine; sodium acetate 1.) glacial acetic acid, acetic anhydride, reflux, 1 h, 2.) glacial acetic acid, acetic anhydride, 2 h; Yield given. Multistep reaction;
参考文献
Dyke, Hazel J.; Elix, John A.; Marcuccio, Sebastian M.; Whitton, Andrew A.
Australian Journal of Chemistry, 1987 , vol. 40, # 2 p. 431 - 434
参考文献
Koller; Pfeiffer
Monatshefte fuer Chemie, 1933 , vol. 62, p. 359,370, 371
参考文献
Asahina; Akagi
Chemische Berichte, 1935 , vol. 68, p. 1130,1132
Yakugaku Zasshi, 1935 , vol. 55, p. 1117,1121
反应条件
lithium diisopropyl amide T=15°C; 1 h; other reagents, time, temperature; Product distribution;
参考文献
Barrett, Anthony G. M.; Morris, Timothy M.; Barton, Derek H. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2272 - 2277
反应条件
methanol 20 h; Heating;
参考文献
Sakurai, Atsushi; Goto, Yohko
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 5 p. 1917 - 1918
反应条件
sodium hydrogencarbonate; acetone
参考文献
Saraiya; Shah
Proceedings - Indian Academy of Sciences, Section A, 1950 , vol. <A> 31, p. 187,189
反应条件
acetone; silver(l) oxide Behandeln des Reaktionsprodukts mit methanol. Kalilauge;
参考文献
Robertson; Stephenson
Journal of the Chemical Society, 1932 , p. 1388,1393
反应条件
lithium diisopropyl amide 1.) 6 h, room temperature, 2.) pH 9.2 buffer, overnight; Yield given. Multistep reaction;
参考文献
Barrett, Anthony G. M.; Morris, Timothy M.; Barton, Derek H. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2272 - 2277
反应条件
lithium diisopropyl amide 1.) 3 h, room temperature, 2.) pH 9.2 buffer, overnight; Yield given. Multistep reaction;
参考文献
Barrett, Anthony G. M.; Morris, Timothy M.; Barton, Derek H. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2272 - 2277