2,4-二羟基-6-甲基苯甲酸甲酯合成路线 （共 72 条）
反应条件
sodium hydride 1.) -60 deg C --> room temperature, 6 h, tetrahydrofuran, 2.) benzene, reflux; Yield given. Multistep reaction;
参考文献
Jaxa-Chamiec, Albert A.; Sammes, Peter G.; Kennewell, Peter D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 170 - 175
反应条件
lithium diisopropyl amide 1.) 3 h, room temperature, 2.) pH 9.2 buffer, overnight; Yield given. Multistep reaction;
参考文献
Barrett, Anthony G. M.; Morris, Timothy M.; Barton, Derek H. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2272 - 2277
参考文献
Spaeth; Jeschki
Chemische Berichte, 1924 , vol. 57, p. 473
参考文献
Lopes, Thiago Inacio Barros; Coelho, Roberta Gomes; Yoshida, Nidia Cristiane; Honda, Neli Kika
Chemical and Pharmaceutical Bulletin, 2008 , vol. 56, # 11 p. 1551 - 1554
反应条件
titanium tetrachloride in dichloromethane -78 deg C -> room temperature;
参考文献
Just, George; Sacripante, Guerino; Zamir, Lolita
Synthetic Communications, 1985 , vol. 15, # 11 p. 1007 - 1012
参考文献
Huneck, Siegfried
Phytochemistry (Elsevier), 1984 , vol. 23, # 11 p. 2697 - 2698
参考文献
Herzig; Wenzel; Kurzweil
Monatshefte fuer Chemie, 1903 , vol. 24, p. 898
参考文献
Stenhouse
Justus Liebigs Annalen der Chemie, 1848 , vol. 68, p. 61,68
Justus Liebigs Annalen der Chemie, 1869 , vol. 149, p. 289
Full Text Show Details
Strecker
Justus Liebigs Annalen der Chemie, 1848 , vol. 68, p. 111,113
反应条件
titanium tetrachloride in dichloromethane influence of the ratio of reagents and temperature; Product distribution;
参考文献
Just, George; Sacripante, Guerino; Zamir, Lolita
Synthetic Communications, 1985 , vol. 15, # 11 p. 1007 - 1012
参考文献
Donnelly, Dervilla; Sanada, Shuichi; O'Reilly, Joseph; Polonsky, Judith; Prange, Thierry; Pascard, Claudine
Journal of the Chemical Society, Chemical Communications, 1982 , # 2 p. 135 - 137
