2,4-二羟基-6-甲基苯甲酸甲酯合成路线 （共 72 条）
反应条件
diethyl ether Einleiten von Chlorwasserstoff; Erwaermen des Reaktionsprodukts mit Wasser;
参考文献
Curd; Robertson; Stephenson
Journal of the Chemical Society, 1933 , p. 130,132
Full Text Show Details
Fujikawa; Nakamura
Yakugaku Zasshi, 1942 , vol. 62, p. 304,306; dtsch. Ref. S. 82
Chem.Abstr., 1951 , p. 583
反应条件
diethyl ether Einleiten von Chlorwasserstoff; Erwaermen des Reaktionsprodukts mit Wasser;
参考文献
Curd; Robertson; Stephenson
Journal of the Chemical Society, 1933 , p. 130,132
Full Text Show Details
Fujikawa; Nakamura
Yakugaku Zasshi, 1942 , vol. 62, p. 304,306; dtsch. Ref. S. 82
Chem.Abstr., 1951 , p. 583
反应条件
1: 80 percent / AlCl3 / diethyl ether 2: 78 percent / Zn(Hg); HCl / methanol 3: 90 percent / CF3COOH View Scheme
参考文献
Ponde, Datta E.; Ramalingam; Patil, Mahesh L.; Borate, Hanumant B.; Deshpande, Vishnu H.
Tetrahedron Letters, 1999 , vol. 40, # 29 p. 5399 - 5400
反应条件
1: 56 percent / pyridine / CH2Cl2 / 48 h / -10 °C 2: 66 percent / K2CO3 / 1,2-dimethoxy-ethane / 24 h / Heating 3: 74 percent / NaOCH3 / methanol / 168 h / 20 °C View Scheme
参考文献
Dornhagen, Juergen; Scharf, Hans-Dieter
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1985 , vol. 40, # 11 p. 1541 - 1549
反应条件
1: K2CO3 / acetone / Heating
2: 99 percent / KOH / ethanol
View Scheme
参考文献
Fuerstner, Alois; Castanet, Anne-Sophie; Radkowski, Karin; Lehmann, Christian W.
Journal of Organic Chemistry, 2003 , vol. 68, # 4 p. 1521 - 1528
反应条件
1: K2CO3 / acetone / Heating
2: 99 percent / KOH / ethanol
3: LDA
4: K2CO3
View Scheme
参考文献
Fuerstner, Alois; Castanet, Anne-Sophie; Radkowski, Karin; Lehmann, Christian W.
Journal of Organic Chemistry, 2003 , vol. 68, # 4 p. 1521 - 1528
反应条件
1: 64 percent / NaOMe / methanol / 5 h / 65 °C
2: 96 percent / iodine; aq. H2O2 / ethanol
View Scheme
参考文献
Drochner, Daniel; Huettel, Wolfgang; Bode, Silke E.; Mueller, Michael; Karl, Ulrich; Nieger, Martin; Steglich, Wolfgang
European Journal of Organic Chemistry, 2007 , # 11 p. 1749 - 1758
反应条件
1: concentrated sulfuric acid
2: aqueous KOH-solution
3: quinoline; copper-powder
View Scheme
参考文献
Saraiya; Shah
Proceedings - Indian Academy of Sciences, Section A, 1950 , # 31 p. 213,217
反应条件
diethyl ether
Einleiten von Chlorwasserstoff; Erwaermen des Reaktionsprodukts mit Wasser;
参考文献
Curd; Robertson; Stephenson
Journal of the Chemical Society, 1933 , p. 130,132
Full Text Show Details
Fujikawa; Nakamura
Yakugaku Zasshi, 1942 , vol. 62, p. 304,306; dtsch. Ref. S. 82
Chem.Abstr., 1951 , p. 583
反应条件
diethyl ether
Einleiten von Chlorwasserstoff; Erwaermen des Reaktionsprodukts mit Wasser;
参考文献
Curd; Robertson; Stephenson
Journal of the Chemical Society, 1933 , p. 130,132
Full Text Show Details
Fujikawa; Nakamura
Yakugaku Zasshi, 1942 , vol. 62, p. 304,306; dtsch. Ref. S. 82
Chem.Abstr., 1951 , p. 583
