in dichloromethane (Ar); a soln. of ruthenium and iron complexes in CH2Cl2 was heated under reflux for 3 h; evapn.; column chromy. (SiO2, CH2Cl2 or CH2Cl2/ethyl acetate); recrystn.;
参考文献
Journal of Organometallic Chemistry, , vol. 610, # 1-2 p. 31 - 37
in dichloromethane
(Ar); a soln. of ruthenium and iron complexes in CH2Cl2 was heated under reflux for 3 h; evapn.; column chromy. (SiO2, CH2Cl2 or CH2Cl2/ethyl acetate); recrystn.;
参考文献
Katayama, Taku; Onitsuka, Kiyotaka; Takahashi, Shigetoshi
Journal of Organometallic Chemistry, 2000 , vol. 610, # 1-2 p. 31 - 37
in dichloromethane
(Ar); soln. of Ru complex and Fe complex in CH2Cl2 was refluxed for 3 h; solvent removed; chromd. (silica gel, CH2Cl2 or CH2Cl2/EtOAc); recrystd.(CH2Cl2/hexane); elem. anal.;
参考文献
Katayama, Taku; Onitsuka, Kiyotaka; Takahashi, Shigetoshi
Journal of Organometallic Chemistry, 2006 , vol. 691, # 10 p. 2245 - 2256
in dichloromethane
(Ar); soln. of Ru complex and Fe complex in CH2Cl2 was refluxed for 3 h; solvent removed; chromd. (silica gel, CH2Cl2 or CH2Cl2/EtOAc); recrystd.(CH2Cl2/hexane); elem. anal.;
参考文献
Katayama, Taku; Onitsuka, Kiyotaka; Takahashi, Shigetoshi
Journal of Organometallic Chemistry, 2006 , vol. 691, # 10 p. 2245 - 2256
