反应条件
1: 96 percent / aq. acetic acid / 15 h / Ambient temperature
2: 97 percent / NaH / tetrahydrofuran / 0 °C
3: 1.) t-BuLi, 2.) Cl3CCCl3 / 1.) ether, pentane, -78 deg C, 20 min, 0 deg C, 1 h, 2.) ether, pentane, -78 deg C to rt
4: benzene / Ambient temperature
5: 3.46 g / TBAF / tetrahydrofuran / 1 h
6: 99 percent / NaH / tetrahydrofuran / 0.5 h / 0 °C
7: 52 percent / BH3*THF / tetrahydrofuran / 16 h / Ambient temperature; other solvent, reagent, temperature, reaction time
8: 54 percent / LDA / tetrahydrofuran / -50 - 0 °C / other reagent, temperature, reaction time
9: O2, salcomine / dimethylformamide / 2 h / Ambient temperature
10: NH4Cl / methanol / 13 h / Ambient temperature
View Scheme
参考文献
Iwao, Masatomo; Motoi, Osamu; Fukuda, Tsutomu; Ishibashi, Fumito
Tetrahedron, 1998 , vol. 54, # 31 p. 8999 - 9010
