3,3,3,-三氟-2-(三氟甲基)-1,2-氧化丙烯合成路线 (共 13 条)
反应条件
sodium hypochlorite; Aliquatreg; 336 T=-5 - 2°C; 1.5 - 2 h;
参考文献
E.I. DU PONT DE NEMOURS AND COMPANY
Patent: EP1177184 B1, 2004 ;
Location in patent: Page 3 ;
反应条件
sodium hypochlorite; Aliquatreg; 336 T=-2 - 2°C; 2 h;
参考文献
Petrov, Viacheslav A.
Journal of Fluorine Chemistry, 2004 , vol. 125, # 4 p. 531 - 536
反应条件
sodium hydroxide in water 1 h; Cooling with ice;
参考文献
US2013/5997 A1, ;
Page/Page column 7 ;
反应条件
oxygen T=230°C; P=10343.2 Torr; 12 h; Product distribution / selectivity;
参考文献
US2008/177097 A1, ;
Page/Page column 1-2 ;
反应条件
in diethyl ether T=20°C; 6 h;
参考文献
Chemistry - A European Journal, , vol. 13, # 3 p. 923 - 935
反应条件
water in tetrahydrofuran T=175°C; 12 h;
参考文献
Petrov, Viacheslav A.
Synthesis, 2002 , # 15 p. 2225 - 2231
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in diethyl ether T=10 - 25°C; 20 h;
参考文献
Petrov, Viacheslav A.
Journal of Fluorine Chemistry, 2004 , vol. 125, # 4 p. 531 - 536
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in diethyl ether T=10 - 25°C; 16 h;
参考文献
Petrov, Viacheslav A.
Journal of Fluorine Chemistry, 2004 , vol. 125, # 4 p. 531 - 536
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in diethyl ether T=10 - 25°C; 20 h;
参考文献
Petrov, Viacheslav A.
Journal of Fluorine Chemistry, 2004 , vol. 125, # 4 p. 531 - 536
反应条件
aluminium trichloride T=10°C; 1 h;
参考文献
Petrov, Viacheslav A.
Synthesis, 2002 , # 15 p. 2225 - 2231