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乙二醇
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63148-62-9
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二甲基亚砜
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471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
31910-65-3
合成路线
（共 17 条）
880104-82-5
→
反应条件
31910-65-3
反应条件
2,2'-azo-bisisobutyronitrile; tris-(trimethylsilyl)silane in benzene Heating;
参考文献
Coulomb, Julien; Certal, Victor; Larraufie, Marie-Helene; Ollivier, Cyril; Corbet, Jean-Pierre; Mignani, Gerard; Fensterbank, Louis; Lacote, Emmanuel; Malacria, Max
Chemistry - A European Journal, 2009 , vol. 15, # 39 p. 10225 - 10232
880104-81-4
→
反应条件
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene Heating;
参考文献
Coulomb, Julien; Certal, Victor; Larraufie, Marie-Helene; Ollivier, Cyril; Corbet, Jean-Pierre; Mignani, Gerard; Fensterbank, Louis; Lacote, Emmanuel; Malacria, Max
Chemistry - A European Journal, 2009 , vol. 15, # 39 p. 10225 - 10232
5159-41-1
2-碘苄醇
→
反应条件
31910-65-3
反应条件
1: 96 percent / pyridine / CH2Cl2 / 0.17 h / 0 °C 2: 97 percent / AIBN; Bu3SnH / benzene / Heating View Scheme
参考文献
Coulomb, Julien; Certal, Victor; Fensterbank, Louis; Lacote, Emmanuel; Malacria, Max
Angewandte Chemie - International Edition, 2006 , vol. 45, # 4 p. 633 - 637
1198104-46-9
→
反应条件
31910-65-3
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene 1 h; Reflux;
参考文献
Coulomb, Julien; Certal, Victor; Larraufie, Marie-Helene; Ollivier, Cyril; Corbet, Jean-Pierre; Mignani, Gerard; Fensterbank, Louis; Lacote, Emmanuel; Malacria, Max
Chemistry - A European Journal, 2009 , vol. 15, # 39 p. 10225 - 10232
1198104-47-0
→
反应条件
31910-65-3
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene 1 h; Reflux;
参考文献
Coulomb, Julien; Certal, Victor; Larraufie, Marie-Helene; Ollivier, Cyril; Corbet, Jean-Pierre; Mignani, Gerard; Fensterbank, Louis; Lacote, Emmanuel; Malacria, Max
Chemistry - A European Journal, 2009 , vol. 15, # 39 p. 10225 - 10232
1198104-48-1
→
反应条件
31910-65-3
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene 1 h; Reflux;
参考文献
Coulomb, Julien; Certal, Victor; Larraufie, Marie-Helene; Ollivier, Cyril; Corbet, Jean-Pierre; Mignani, Gerard; Fensterbank, Louis; Lacote, Emmanuel; Malacria, Max
Chemistry - A European Journal, 2009 , vol. 15, # 39 p. 10225 - 10232
1198104-49-2
→
反应条件
31910-65-3
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene 1 h; Reflux;
参考文献
Coulomb, Julien; Certal, Victor; Larraufie, Marie-Helene; Ollivier, Cyril; Corbet, Jean-Pierre; Mignani, Gerard; Fensterbank, Louis; Lacote, Emmanuel; Malacria, Max
Chemistry - A European Journal, 2009 , vol. 15, # 39 p. 10225 - 10232
880104-81-4
→
反应条件
反应条件
triethyl borane; tri-n-butyl-tin hydride in toluene T=20°C;
参考文献
Coulomb, Julien; Certal, Victor; Larraufie, Marie-Helene; Ollivier, Cyril; Corbet, Jean-Pierre; Mignani, Gerard; Fensterbank, Louis; Lacote, Emmanuel; Malacria, Max
Chemistry - A European Journal, 2009 , vol. 15, # 39 p. 10225 - 10232
18982-54-2
2-溴苄醇
→
反应条件
31910-65-3
反应条件
n-butyllithium; sulfur dioxide in tetrahydrofuran 1.) -78 degC to 0 deg C, 30 min; 2.) -78 deg C;
参考文献
Durst, Tony; Charlton, James L.; Mount, David B.
Canadian Journal of Chemistry, 1986 , vol. 64, p. 246 - 249
880104-81-4
→
反应条件
31910-65-3
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene 3 h; Reflux;
参考文献
Coulomb, Julien; Certal, Victor; Larraufie, Marie-Helene; Ollivier, Cyril; Corbet, Jean-Pierre; Mignani, Gerard; Fensterbank, Louis; Lacote, Emmanuel; Malacria, Max
Chemistry - A European Journal, 2009 , vol. 15, # 39 p. 10225 - 10232
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