N-甲基-N-乙烯基乙酰胺合成路线 (共 18 条)
反应条件
1: With trifluoroacetic acid 2: With water
参考文献
Prashad, Mahavir; Lu, Yansong; Repic, Oljan
Journal of Organic Chemistry, 2004 , vol. 69, # 2 p. 584 - 586
参考文献
Kadaba
Journal of Organic Chemistry, 1992 , vol. 57, # 11 p. 3075 - 3078
反应条件
sodium hydroxide; sodium tetrahydroborate; mercury(II) diacetate 1.) THF, 0 deg C, H2O, 15 min; Yield given. Multistep reaction;
参考文献
Inaba, Masami; Moriwake, Toshio; Saito, Seiki
Tetrahedron Letters, 1985 , vol. 26, # 27 p. 3235 - 3238
反应条件
1: With trifluoroacetic acid 2: With water
参考文献
Prashad, Mahavir; Lu, Yansong; Repic, Oljan
Journal of Organic Chemistry, 2004 , vol. 69, # 2 p. 584 - 586
反应条件
acetic acid in ethyl acetate
T=20°C;
参考文献
Garcia, Alberto; Gomez, Eduardo; Dominguez, Domingo
Synlett, 2004 , # 13 p. 2331 - 2334
反应条件
[Ru(η6-1,3,5-cyclooctatriene)(η2-dimethyl fumarate)2] in N,N-dimethyl acetamide
T=160°C; 3 h;
参考文献
Tsujita, Hiroshi; Ura, Yasuyuki; Matsuki, Shingo; Wada, Kenji; Mitsudo, Take-Aki; Kondo, Teruyuki
Angewandte Chemie - International Edition, 2007 , vol. 46, # 27 p. 5160 - 5163
反应条件
[Ru(.eta.6-(1,3,5-cyclooctatriene))(dimethylfumarate)2] in isobutyramide
T=160°C; 1 - 3 h; Product distribution / selectivity;
参考文献
Kyoto University
Patent: WO2007/26654 A1, 2007 ;
Location in patent: Page/Page column 15-17; 19; 21 ;
反应条件
anhydrous iron chloride in dichloromethane
T=40°C; 1 h;
参考文献
Niu, Tianmin; Huang, Lehao; Wu, Tianxing; Zhang, Yuhong
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 1 p. 273 - 277