2-(1-环己烯基)乙醇合成路线 （共 33 条）
反应条件
thallium(III) nitrate in pentane
T=20°C; Oxidation; Rearragement; Cyclization; 48 h;
参考文献
Ferraz, Helena M. C.; Santos, Andrea P.; Silva Jr., Luiz F.; Vieira, Tiago De O.
Synthetic Communications, 2000 , vol. 30, # 4 p. 751 - 762
反应条件
1: m-CPBA / CH2Cl2
2: 88 percent / AlEt3 / tetrahydrofuran / 40 °C
View Scheme
参考文献
Wang, Fei; Wang, Shao Hua; Tu, Yong Qiang; Ren, Shi Kuo
Tetrahedron Asymmetry, 2003 , vol. 14, # 15 p. 2189 - 2193
反应条件
1: 71 percent / pyridine / 24 h / 0 - 5 °C
2: 54 percent / NaI / acetone / 24 h / Heating
3: 94 percent / NaCN / 72 h / 80 °C
4: 84 percent / KOH / ethanol; H2O / 18 h / 80 - 90 °C
5: 98 percent / LiAlH4 / diethyl ether / 18 h / 20 °C
6: 73 percent / pyridine / 48 h / 0 °C
View Scheme
参考文献
Crotti, Paolo; Badalassi, Fabrizio; Di Bussolo, Valeria; Favero, Lucilla; Pineschi, Mauro
Tetrahedron, 2001 , vol. 57, # 40 p. 8559 - 8572
