2-溴-7-碘-9,9-二甲基芴合成路线 （共 3 条）
反应条件
sulfuric acid; iodine; acetic acid; periodic acid in water T=50°C; 5 h;
参考文献
Samsung Mobile Display Co., Ltd.
Patent: EP2292603 A1, 2011 ;
Location in patent: Page/Page column 24 ;
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in water; dimethyl sulfoxide 5 h;
参考文献
WO2006/114921 A1, ;
Page/Page column 74-77 ;
反应条件
1: 2-bromo-7-iodo-9,9-dimethylfluorene With n-butyllithium in tetrahydrofuran; hexane
T=-65°C; 0.5 h; Inert atmosphere;
2: N,N-dimethyl-formamide in tetrahydrofuran; hexane
T=-65 - 20°C;
参考文献
Idemitsu Kosan Co., Ltd.
Patent: EP2351759 A1, 2011 ;
Location in patent: Page/Page column 33 ;
