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63148-62-9
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471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
319906-47-3
合成路线
（共 10 条）
111-25-1
溴已烷
+
123348-27-6
2-溴-7-碘芴
→
反应条件
319906-47-3
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in dimethyl sulfoxide T=20°C; 15 h;
参考文献
Promarak, Vinich; Punkvuang, Auradee; Sudyoadsuk, Taweesak; Jungsuttiwong, Siriporn; Saengsuwan, Sayant; Keawin, Tinnagon; Sirithip, Karnokkorn
Tetrahedron, 2007 , vol. 63, # 36 p. 8881 - 8890
226070-05-9
9,9-二己基-2-溴芴
→
反应条件
319906-47-3
反应条件
sulfuric acid; iodine; periodic acid in water; acetic acid T=80°C; 12 h;
参考文献
Cheng, Yen-Ju; Hung, Lung-Chang; Cao, Fong-Yi; Kao, Wei-Shun; Chang, Chih-Yu; Hsu, Chain-Shu
Journal of Polymer Science, Part A: Polymer Chemistry, 2011 , vol. 49, # 8 p. 1791 - 1801
1262414-52-7
→
反应条件
319906-47-3
反应条件
1: With hydrogenchloride; sodium nitrite in water T=0°C; 1 h; 2: With potassium iodide in water T=20°C;
参考文献
Lin, Tzu-Chau; Liu, Che-Yu; Huang, Bor-Rong; Lin, Ja-Hon; Shen, Yu-Kai; Wu, Cheng-Yu
European Journal of Organic Chemistry, 2013 , # 3 p. 498 - 508
1133-80-8
2-溴芴
→
反应条件
319906-47-3
反应条件
1: 80 percent / AcOH; KIO3; I2 / aq. H2SO4 / 20 h / 80 °C 2: 94 percent / triethylbenzylammonium chloride; aq. NaOH / dimethylsulfoxide / 15 h / 20 °C View Scheme
参考文献
Linton, Katharine E.; Fisher, Alison L.; Pearson, Christopher; Fox, Mark A.; Palsson, Lars-Olof; Bryce, Martin R.; Petty, Michael C.
Journal of Materials Chemistry, 2012 , vol. 22, # 23 p. 11816 - 11825
111-25-1
溴已烷
→
反应条件
319906-47-3
反应条件
1: tetrabutylammomium bromide; sodium hydroxide / tetrahydrofuran; water / 12 h / 80 °C / Inert atmosphere 2: sulfuric acid; iodine; periodic acid / water; acetic acid / 12 h / 80 °C View Scheme
参考文献
Lin, Tzu-Chau; Liu, Che-Yu; Huang, Bor-Rong; Lin, Ja-Hon; Shen, Yu-Kai; Wu, Cheng-Yu
European Journal of Organic Chemistry, 2013 , # 3 p. 498 - 508
123863-97-8
9,9-二己基芴
→
反应条件
319906-47-3
反应条件
1.1: nitric acid / acetic acid / 0.25 h / 10 °C 2.1: zinc(II) chloride; benzyltrimethylammonium bromide dibromide / acetic acid / 6 h / |Reflux 3.1: SnCl2·2H2O / ethyl acetate / 6 h / |Reflux 4.1: hydrogenchloride; sodium nitrite / water / 1 h / 0 °C 4.2: 20 °C View Scheme
参考文献
Lin, Tzu-Chau; Liu, Che-Yu; Huang, Bor-Rong; Lin, Ja-Hon; Shen, Yu-Kai; Wu, Cheng-Yu
European Journal of Organic Chemistry, 2013 , # 3 p. 498 - 508
86-73-7
芴
→
反应条件
319906-47-3
反应条件
1.1: potassium iodide; sodium t-butanolate / tetrahydrofuran / 1 h / |Reflux 1.2: |Reflux 2.1: nitric acid / acetic acid / 0.25 h / 10 °C 3.1: zinc(II) chloride; benzyltrimethylammonium bromide dibromide / acetic acid / 6 h / |Reflux 4.1: SnCl2·2H2O / ethyl acetate / 6 h / |Reflux 5.1: hydrogenchloride; sodium nitrite / water / 1 h / 0 °C 5.2: 20 °C View Scheme
参考文献
Lin, Tzu-Chau; Liu, Che-Yu; Huang, Bor-Rong; Lin, Ja-Hon; Shen, Yu-Kai; Wu, Cheng-Yu
European Journal of Organic Chemistry, 2013 , # 3 p. 498 - 508
1182371-73-8
→
反应条件
319906-47-3
反应条件
1.1: zinc(II) chloride; benzyltrimethylammonium bromide dibromide / acetic acid / 6 h / |Reflux 2.1: SnCl2·2H2O / ethyl acetate / 6 h / |Reflux 3.1: hydrogenchloride; sodium nitrite / water / 1 h / 0 °C 3.2: 20 °C View Scheme
参考文献
Lin, Tzu-Chau; Liu, Che-Yu; Huang, Bor-Rong; Lin, Ja-Hon; Shen, Yu-Kai; Wu, Cheng-Yu
European Journal of Organic Chemistry, 2013 , # 3 p. 498 - 508
865152-23-4
→
反应条件
319906-47-3
反应条件
1.1: SnCl2·2H2O / ethyl acetate / 6 h / |Reflux 2.1: hydrogenchloride; sodium nitrite / water / 1 h / 0 °C 2.2: 20 °C View Scheme
参考文献
Lin, Tzu-Chau; Liu, Che-Yu; Huang, Bor-Rong; Lin, Ja-Hon; Shen, Yu-Kai; Wu, Cheng-Yu
European Journal of Organic Chemistry, 2013 , # 3 p. 498 - 508
319906-42-8
→
反应条件
319906-47-3
反应条件
暂无反应条件数据
参考文献
Liu, Wen-Jun; Zhou, Yan; Zhou, Qi-Feng; Ma, Yuguo; Pei, Jian
Organic Letters, 2008 , vol. 10, # 11 p. 2123 - 2126
