2,5-二(三氟甲基)硝基苯合成路线 （共 8 条）
反应条件
sulfuric acid; sulfur trioxide; nitric acid T=80°C; 8 - 10 h;
参考文献
ASAHI GLASS COMPANY LTD.
Patent: EP1468983 A1, 2004 ;
Location in patent: Page 6 ;
反应条件
isobutyramide; copper T=100°C; 8 h;
参考文献
Journal of Fluorine Chemistry, , vol. 50, # 3 p. 411 - 426
反应条件
copper in N,N-dimethyl acetamide T=100°C; 4 h; with or without charcoal; Product distribution;
参考文献
Clark, James H.; McClinton, Martin A.; Jones, Craig W.; Landon, Philip; Bishop, D.; Blade, R. J.
Tetrahedron Letters, 1989 , vol. 30, # 16 p. 2133 - 2136
反应条件
potassium fluoride; copper(l) iodide in N,N-dimethyl-formamide T=100 - 110°C; 10 h; Yield given;
参考文献
Journal of Fluorine Chemistry, , vol. 66, # 2 p. 167 - 170
反应条件
potassium fluoride; copper(l) iodide in N,N-dimethyl-formamide T=90°C; 8 h; Yield given;
参考文献
Journal of Fluorine Chemistry, , vol. 66, # 2 p. 167 - 170
反应条件
copper(l) iodide in N,N-dimethyl-formamide T=70 - 80°C; 10 h; Yield given;
参考文献
Journal of Fluorine Chemistry, , vol. 66, # 2 p. 167 - 170
反应条件
hydrogen; nickel in isopropyl alcohol T=70 - 90°C; P=3677.86 Torr; 8 h;
参考文献
ASAHI GLASS COMPANY LTD.
Patent: EP1468983 A1, 2004 ;
Location in patent: Page 6 ;
反应条件
1: SnCl2+2H2O; concentrated HCl 2: aqueous hydrochloric acid; sodium nitrite; sodium iodide View Scheme
参考文献
Ross et al.
Journal of the American Chemical Society, 1953 , vol. 75, p. 4967
