2-N-boc-2-甲基-1,2-丙二胺合成路线 (共 4 条)
反应条件
palladium 10 on activated carbon; hydrogen in methanol T=20°C; 0.5 h;
参考文献
Fremaux, Juliette; Dolain, Christel; Kauffmann, Brice; Clayden, Jonathan; Guichard, Gilles
Chemical Communications, 2013 , vol. 49, # 67 p. 7415 - 7417
反应条件
hydrazine hydrate in ethanol; dichloromethane T=20°C;
参考文献
Hunt, Thomas; Atherton-Watson, Hazel C.; Collingwood, Stephen P.; Coote, Kevin J.; Czarnecki, Sarah; Danahay, Henry; Howsham, Catherine; Hunt, Peter; Paisley, Derek; Young, Alice
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 8 p. 2877 - 2879
反应条件
1: triethylamine / dichloromethane / 20 °C 2: triphenylphosphine; diethylazodicarboxylate / dichloromethane / 20 °C 3: hydrazine hydrate / ethanol; dichloromethane / 20 °C View Scheme
参考文献
Fremaux, Juliette; Dolain, Christel; Kauffmann, Brice; Clayden, Jonathan; Guichard, Gilles
Chemical Communications, 2013 , vol. 49, # 67 p. 7415 - 7417
反应条件
1: triphenylphosphine; diethylazodicarboxylate / dichloromethane / 20 °C 2: hydrazine hydrate / ethanol; dichloromethane / 20 °C View Scheme
参考文献
Hunt, Thomas; Atherton-Watson, Hazel C.; Collingwood, Stephen P.; Coote, Kevin J.; Czarnecki, Sarah; Danahay, Henry; Howsham, Catherine; Hunt, Peter; Paisley, Derek; Young, Alice
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 8 p. 2877 - 2879