(Z)-1-偶氮基-4-[(4-甲基苯基)磺酰基氨基]丁-1-烯-2-醇合成路线 （共 7 条）
反应条件
in diethyl ether T=-15 - -10°C;
参考文献
Sajadi; Kashani; Loeffler; Hall
Journal of Medicinal Chemistry, 1980 , vol. 23, # 3 p. 275 - 278
反应条件
1: (COCl)2, DMF / CH2Cl2 / 3 h / Ambient temperature 2: tetrahydrofuran; diethyl ether / 4 h / 0 - 20 °C View Scheme
参考文献
Wang, Jianbo; Hou, Yihua
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 12 p. 1919 - 1923
反应条件
styrene; copper acetylacetonate in benzene Cyclization; Heating;
参考文献
Wang, Jianbo; Hou, Yihua; Wu, Peng
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 16 p. 2277 - 2280
反应条件
copper acetylacetonate; tri-n-butyl-tin hydride in benzene Cyclization; reduction; 5 h; Heating;
参考文献
Tetrahedron, , vol. 56, # 38 p. 7457 - 7461
反应条件
silver benzoate; triethylamine in tetrahydrofuran 2 h; Ambient temperature;
参考文献
Wang, Jianbo; Hou, Yihua
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 12 p. 1919 - 1923
反应条件
tri-n-butyl-tin hydride in benzene
T=20°C; Reduction; Irradiation;
参考文献
Tan, Zhongping; Qu, Zhaohui; Chen, Bei; Wang, Jianbo
Tetrahedron, 2000 , vol. 56, # 38 p. 7457 - 7461
反应条件
copper acetylacetonate; tri-n-butyl-tin hydride in benzene
Cyclization; reduction; 5 h; Heating;
参考文献
Tan, Zhongping; Qu, Zhaohui; Chen, Bei; Wang, Jianbo
Tetrahedron, 2000 , vol. 56, # 38 p. 7457 - 7461
