1: With n-butyllithium in tetrahydrofuran; hexane T=0°C; Flow reactor; 2: With N-fluoro-N-(phenylsulfonyl)benzene-sulfonamide in tetrahydrofuran; hexane T=0°C; Flow reactor; Reagent/catalyst;
参考文献
Chemistry - An Asian Journal, , vol. 8, # 4 p. 705 - 708
1: With Bu4MgLi2 in tetrahydrofuran; hexane RefluxInert atmosphere; 2: With N-fluorobenzene sulfonamide in tetrahydrofuran; hexane T=20°C; Inert atmosphere;
参考文献
Chemical Communications, , vol. 46, # 37 p. 7043 - 7045
1-chloromethyl-4-fluoro-1,4-diazonia-bicyclolt;2.2.2gt;octane ditriflate in acetonitrile T=90°C; Yield given. Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 16 p. 2069 - 2076