反应条件
1: 4-fluoro-l-naphthalene; (s)-(-)-N,N-dimethyl-3-(thien-2-yl)-3-hydroxy-propanamine With tetrabutylammomium bromide; sodium hydroxide in dimethyl sulfoxide T=50 - 65°C; 2: oxalic acid in toluene T=55 - 60°C; 1 h; optical yield given as percent eeenantioselective reaction;
参考文献
Suthrapu, Sashikanth; Sripathi, Somaiah; Veeramalla, Raju; Bojja, Ramachandra Reddy; Karnati, Venugopal Reddy
Organic Process Research and Development, 2009 , vol. 13, # 5 p. 854 - 856