2-羟基-2,4-二甲基-3-戊酮合成路线 （共 13 条）
参考文献
Colonge,J.; Dubin,J.-C.
Bulletin de la Societe Chimique de France, 1960 , p. 1180 - 1186
参考文献
Blaise; Herman
Annales de Chimie (Cachan, France), 1910 , vol. <8>20, p. 175
Full Text Show Details
Blaise; Herman
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1908 , vol. 146, p. 480
Annales de Chimie (Cachan, France), 1909 , vol. <8>17, p. 388
反应条件
1: Br2 / 1 h / 5 - 10 °C
2: DBU / dimethylformamide / 2 h / Ambient temperature
3: 70 percent / Et3N, DMAP / CH2Cl2 / 4 h / 0 °C
4: 10 percent / diethyl ether; various solvent(s) / 0.5 h / -78 °C
5: 82 percent / diethyl ether; various solvent(s) / 0.5 h / -78 °C
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参考文献
Barbee, Thomas R.; Albizati, Kim F.
Journal of Organic Chemistry, 1991 , vol. 56, # 24 p. 6764 - 6773
