2,4-二甲基-1-戊烯-3-酮合成路线 （共 26 条）
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in N,N-dimethyl-formamide 2 h; Ambient temperature;
参考文献
Barbee, Thomas R.; Albizati, Kim F.
Journal of Organic Chemistry, 1991 , vol. 56, # 24 p. 6764 - 6773
反应条件
hydrogenchloride in N-methyl-acetamide
参考文献
Quest International B.V.
Patent: US6559118 B1, 2003 ;
参考文献
Colonge,J.; Dubin,J.-C.
Bulletin de la Societe Chimique de France, 1960 , p. 1180 - 1186
反应条件
(i) (bromination), (ii) Py; Multistep reaction;
参考文献
Yandovskii, V. N.; Gidaspov, B. V.; Telinskii, I. V.
Doklady Chemistry, 1986 , vol. 289, p. 256 - 259
Dokl. Akad. Nauk SSSR Ser. Khim., 1986 , vol. 289, # 1 p. 120 - 123
反应条件
in diethyl ether T=-78°C; 0.5 h;
参考文献
Barbee, Thomas R.; Albizati, Kim F.
Journal of Organic Chemistry, 1991 , vol. 56, # 24 p. 6764 - 6773
反应条件
in water anodic oxidation, 0,10-0,15 A/cm2, 2,2 V;
参考文献
Chkir, Moncef; Lelandais, Daniel; Bacquet, Cathy
Canadian Journal of Chemistry, 1981 , vol. 59, p. 945 - 951
反应条件
sodium hydrogencarbonate
参考文献
Hart; Curtis
Journal of the American Chemical Society, 1957 , vol. 79, p. 931
反应条件
in acetic acid (electrochemical oxidation);
参考文献
Shono,T. et al.
Journal of the American Chemical Society, 1974 , vol. 96, p. 3532 - 3536
反应条件
in diethyl ether T=-78°C; 0.5 h;
参考文献
Barbee, Thomas R.; Albizati, Kim F.
Journal of Organic Chemistry, 1991 , vol. 56, # 24 p. 6764 - 6773
反应条件
1: 45 percent / DBU / dimethylformamide / 2 h / Ambient temperature 2: 40 percent / diethyl ether; various solvent(s) / 0.5 h / -78 °C View Scheme
参考文献
Barbee, Thomas R.; Albizati, Kim F.
Journal of Organic Chemistry, 1991 , vol. 56, # 24 p. 6764 - 6773
