2,4-二甲基-1-戊烯-3-酮合成路线 (共 26 条)
反应条件
1: 70 percent / Et3N, DMAP / CH2Cl2 / 4 h / 0 °C 2: 10 percent / diethyl ether; various solvent(s) / 0.5 h / -78 °C View Scheme
参考文献
Barbee, Thomas R.; Albizati, Kim F.
Journal of Organic Chemistry, 1991 , vol. 56, # 24 p. 6764 - 6773
反应条件
1: DBU / dimethylformamide / 2 h / Ambient temperature 2: 70 percent / Et3N, DMAP / CH2Cl2 / 4 h / 0 °C 3: 10 percent / diethyl ether; various solvent(s) / 0.5 h / -78 °C View Scheme
参考文献
Barbee, Thomas R.; Albizati, Kim F.
Journal of Organic Chemistry, 1991 , vol. 56, # 24 p. 6764 - 6773
反应条件
sodium trifluoroethoxide in various solvent(s) 13680 h;
参考文献
Foehlisch, Baldur; Gehrlach, Eberhard; Henle, Gerhard; Boberlin, Ursula; Herter, Rolf
Journal of Chemical Research, Miniprint, 1991 , p. 1462 - 1492
参考文献
Yandovskii; Tselinskii
Russian Journal of Organic Chemistry, 1997 , vol. 33, # 2 p. 147 - 152
反应条件
dimethylammonium chloride
参考文献
Mellor,J.M.; Webb,C.F.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1974 , p. 17 - 22
反应条件
sodium trifluoroethoxide 96 h; Heating;
参考文献
Foehlisch, Baldur; Gehrlach, Eberhard; Henle, Gerhard; Boberlin, Ursula; Herter, Rolf
Journal of Chemical Research, Miniprint, 1991 , p. 1462 - 1492
反应条件
in pentane Irradiationpyrolysis; Quantum yieldProduct distribution;
参考文献
Adam, Waldemar; Fuss, Andreas; Mazenod, Francois P.; Quast, Helmut
Journal of the American Chemical Society, 1981 , vol. 103, # 4 p. 998 - 1000
参考文献
Colonge,J.; Dubin,J.-C.
Bulletin de la Societe Chimique de France, 1960 , p. 1180 - 1186
反应条件
T=1200°C; pulse pyrolysis; P=1500.15 Torr; Product distribution;
参考文献
Sander, Wolfram; Wrobel, Roman; Komnick, Peter; Rademacher, Paul; Muchall, Heidi M.; Quast, Helmut
European Journal of Organic Chemistry, 2000 , # 1 p. 91 - 98
反应条件
T=1000°C; pyrolysis; P=7.50075E-06 Torr; Product distribution;
参考文献
Sander, Wolfram; Wrobel, Roman; Komnick, Peter; Rademacher, Paul; Muchall, Heidi M.; Quast, Helmut
European Journal of Organic Chemistry, 2000 , # 1 p. 91 - 98