1: With isopropylmagnesium chloride lithium chloride complex in tetrahydrofuran T=0°C; Inert atmosphere; 2: With N-fluoro-N-(phenylsulfonyl)benzene-sulfonamide in dichloromethane; perfluorodecahydronaphthalene T=-78 - 25°C; Inert atmosphere;

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potassium carbonate; cesium fluoride in dimethyl sulfoxide 13 h; Heating;

tetraphenylphosphonium hydrogendifluoride 2 h; Heating;

(i) aq. HCl, NaNO2, NaBF4, (ii) (pyrolysis); Multistep reaction;