1,3-苯并噻唑-2-羧酸乙酯合成路线 （共 33 条）
反应条件
1: cyclobenzothiazole With n-butyllithium in tetrahydrofuran; hexane T=0°C; 2 h; 2: formic acid ethyl ester in tetrahydrofuran; hexane T=-78°C; 3 h; 3: With ethanol; iodine; potassium carbonate in tetrahydrofuran; hexane T=-78 - 20°C; 18 h;
参考文献
Ushijima, Sousuke; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2012 , vol. 68, # 24 p. 4701 - 4709
反应条件
4 h; Heating / reflux;
参考文献
MEDIVIR AB
Patent: WO2008/107365 A1, 2008 ;
Location in patent: Page/Page column 82 ;
WO 2008/107365 A1
反应条件
sodium peroxodisulphate; sulfuric acid; silver nitrate in dichloromethane 1.5 h; Heating;
参考文献
Tetrahedron Letters, , vol. 33, # 21 p. 3057 - 3060
反应条件
[bis(acetoxy)iodo]benzene; water in ethanol T=10°C; 6 h;
参考文献
Prakash, Om; Sharma, Vijay; Sadana, Anil
Journal of Chemical Research - Part S, 1996 , # 2 p. 100 - 101
反应条件
in tetrahydrofuran T=0°C; Substitution;
参考文献
Journal of Organometallic Chemistry, , vol. 588, # 2 p. 155 - 159
反应条件
in ethanol 1.) reflux, 2.5 h, 2.) 1 h;
参考文献
Tetrahedron, , vol. 42, # 10 p. 2625 - 2634
反应条件
[bis(acetoxy)iodo]benzene; water T=10°C; 6 h;
参考文献
Prakash, Om; Sharma, Vijay; Sadana, Anil
Journal of Chemical Research - Part S, 1996 , # 2 p. 100 - 101
参考文献
Liso, Gaetano; Trapani, Giuseppe; Latrofa, Andrea
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 1683 - 1684
反应条件
in toluene 24 h; Heating;
参考文献
Takahashi, Masahiko; Ohba, Masaru
Heterocycles, 1995 , vol. 41, # 3 p. 455 - 460
参考文献
Musser, J. H.; Hudec, T. T.; Bailey, K.
Synthetic Communications, 1984 , vol. 14, # 10 p. 947 - 954
