反应条件
1: 995 mg / aq. NaOH / dioxane; methanol / 2 h / 20 °C 2: 96 percent / H2 / Pd/C / methanol; dioxane / 20 °C 3: 85 percent / K2CO3 / acetone / 0.5 h / Heating 4: 91 percent / K2CO3 / acetone / 0.33 h / Heating 5: TsOH*H2O; AcOH / toluene / 0.75 h / 110 °C 6: 95 percent / BCl3 / CH2Cl2 / 0.25 h / 15 °C 7: 66 percent / aq. NaOH / methanol; dioxane / 1 h / 20 °C View Scheme
参考文献
Tsukayama, Masao; Wada, Hironari; Kawamura, Yasuhiko; Yamashita, Kazuyo; Nishiuchi, Masaki
Chemical and Pharmaceutical Bulletin, 2004 , vol. 52, # 11 p. 1285 - 1289
