5-(4,4,5,5-四甲基-1,3,2-二氧杂硼烷-2-基)嘧啶合成路线 (共 2 条)
反应条件
1: With potassium acetate in dimethyl sulfoxide 0.166667 h; 2: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in dimethyl sulfoxide T=100°C;
参考文献
WO2008/88881 A1, ;
Page/Page column 38 ;
WO 2008/088881 A1
反应条件
bis(η4-1,5-cyclooctadiene)-di-μ-methoxy-diiridium(I); 3,4,7,8-tetra-methyl-1,10-phenanthroline in tetrahydrofuran T=20°C; 25 h; Inert atmosphereGlovebox;
参考文献
Larsen, Matthew A.; Hartwig, John F.
Journal of the American Chemical Society, 2014 , vol. 136, # 11 p. 4287 - 4299