氯化5,10,15,20-四苯基-21H,23H-卟啉镁合成路线 （共 22 条）
反应条件
1: With MnCl2∙4H2O in ethanol 3 h; Reflux; 2: With oxygen in ethanol T=20°C;
参考文献
Eugenia, Fagadar-Cosma; Mirica, Marius Constantin; Balcu, Ionel; Bucovicean, Carmen; Cretu, Carmen; Armeanu, Ileana; Gheorghe, Fagadar-Cosma
Molecules, 2009 , vol. 14, # 4 p. 1370 - 1388
反应条件
in chlorobenzene at 23°C;
参考文献
Journal of the American Chemical Society, , vol. 105, # 11 p. 3510 - 3515
反应条件
N2 in not given metalloporphyrin film on the surface of the single-crystal n-CdSe (buried metalloporphyrin-CdSe surface) was exposed to a flow of N2; not isolated, detected by photoluminescence;
参考文献
Journal of the American Chemical Society, , vol. 122, # 15 p. 3731 - 3738
反应条件
in N,N-dimethyl-formamide 0.5 h; Reflux;
参考文献
Wang, Lanzhi; She, Yuanbin; Zhong, Rugang; Ji, Hongbing; Zhang, Yanhui; Song, Xufeng
Organic Process Research and Development, 2006 , vol. 10, # 4 p. 757 - 761
反应条件
hydrogenchloride in dichloromethane stirred with 1 M aq. HCl; heptane was added, vac.-dried at 100°C;
参考文献
Inorganic Chemistry, , vol. 23, p. 321 - 326
反应条件
in further solvent(s) N2-atmosphere; slight excess Mn-complex, stirring at 140°C for 21h; cooling, collection (filtration), washing (hexane), dissoln. in CH2Cl2, filtration, evapn., repeated extn. with pyridine, washing (CH2Cl2), drying (0.01 Torr, 220°C, 2.5 h); elem. anal.;
参考文献
Donzello, Maria Pia; Ercolani, Claudio; Kadish, Karl M.; Ou, Zhongping; Russo, Umberto
Inorganic Chemistry, 1998 , vol. 37, # 15 p. 3682 - 3688
参考文献
Russian Journal of Physical Chemistry A, , vol. 84, # 9 p. 1631 - 1635
反应条件
hydrogenchloride in methanol; water TPPMn(CH3CO2) dissolved in methanol, addn. of 1 M aq. soln. of HCl, slow addn. of water (dropwise, overnight), ppt.; filtered, dried (vac. oven, 100°C);
参考文献
Canadian Journal of Chemistry, , vol. 67, p. 545 - 550
反应条件
in not given in chlorinated solvents;
参考文献
Inorganic Chemistry, , vol. 25, p. 4668 - 4671
反应条件
in further solvent(s) for 8 h at 120°C in chloronaphthalene;
参考文献
Inorganic Chemistry, , vol. 45, # 17 p. 6988 - 6995
