氯化5,10,15,20-四苯基-21H,23H-卟啉镁合成路线 （共 22 条）
反应条件
in N,N-dimethyl-formamide tetraphenylporphyrin and excess manganese chloride refluxed in DMF for 4h, cooled on ice bath, cold water added to soln. and complex ppd.; FTIR, UV-vis, 1H NMR;
参考文献
Journal of Molecular Catalysis A: Chemical, , vol. 282, # 1-2 p. 149 - 157
反应条件
in chloroform Kinetics; at 288, 298 and 308 K; monitoring by UV;
参考文献
Russian Journal of General Chemistry, , vol. 75, # 6 p. 975 - 979
反应条件
in chloroform Kinetics; at 288, 298 and 308 K; monitoring by UV;
参考文献
Russian Journal of General Chemistry, , vol. 75, # 6 p. 975 - 979
反应条件
in dichloromethane; water; N,N-dimethyl-formamide (N2); Schlenk technique; Mn salt was added to soln. of porphyrin in DMF;stirred under reflux overnight; cooled to room temp.; ice-cooled soln. of NaCl was added; filtered; dissolved in CH2Cl2; satd. soln. of NaCl wa s added; stirred (room temp., 3 h); org. layer septd.; dried (MgSO4); concd. (vac.); chromd. (silica gel, hexane/CH2Cl2, 3/1, 5percent MeOH); evapd.; dried (vac.);
参考文献
Journal of Organometallic Chemistry, , vol. 694, # 14 p. 2153 - 2162
反应条件
in chloroform Kinetics; mixing chloroform solns. of the complexes at 288-308 K; not isolated, detected by UV;
参考文献
Russian Journal of Physical Chemistry A, , vol. 78, # 6 p. 864 - 870
反应条件
in benzonitrile Kinetics; the soln. under anaerobic conditions at 30°C;
参考文献
Yuan, Lung-Chi; Bruice, Thomas C.
Inorganic Chemistry, 1985 , vol. 24, p. 986 - 987
反应条件
in benzonitrile Kinetics; the soln. under anaerobic conditions at 30°C;
参考文献
Yuan, Lung-Chi; Bruice, Thomas C.
Inorganic Chemistry, 1985 , vol. 24, p. 986 - 987
反应条件
in benzonitrile Kinetics; the soln. under anaerobic conditions at 30°C;
参考文献
Yuan, Lung-Chi; Bruice, Thomas C.
Inorganic Chemistry, 1985 , vol. 24, p. 986 - 987
反应条件
in benzonitrile Kinetics; the soln. under anaerobic conditions at 30°C;
参考文献
Inorganic Chemistry, , vol. 24, p. 986 - 987
反应条件
in benzonitrile Kinetics; the soln. under anaerobic conditions at 30°C;
参考文献
Yuan, Lung-Chi; Bruice, Thomas C.
Inorganic Chemistry, 1985 , vol. 24, p. 986 - 987
