(1S)-5-(2-羟基丙-2-基)-2-甲基环己-2-烯-1-醇合成路线 (共 3 条)
反应条件
o-nitrobenzenesulfonyl hydrazide; triphenylphosphine; diethylazodicarboxylate in various solvent(s) -30 deg, 1 h; 23 deg C 30 min;
参考文献
Myers, Andrew G.; Zheng, Bin
Tetrahedron Letters, 1996 , vol. 37, # 28 p. 4841 - 4844
反应条件
3 A molecular sieve; oxygen; (-)-sparteine; Pd((-)-sparteine)2Cl2 in tert-butyl alcohol
T=65°C; 20 h;
参考文献
Mandal, Sunil K.; Sigman, Matthew S.
Journal of Organic Chemistry, 2003 , vol. 68, # 19 p. 7535 - 7537
反应条件
manganese(IV) oxide in chloroform
Ambient temperature; Yield given;
参考文献
Mori, Kenji; Igarashi, Yasuhiro
Liebigs Annalen der Chemie, 1988 , p. 93 - 96