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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
32274-71-8
合成路线
（共 13 条）
63529-06-6
→
反应条件
32274-71-8
反应条件
sulfuric acid in methanol 7 h; Heating;
参考文献
Pouget; Fagnere; Basly; Besson; Champavier; Habrioux; Chulia
Pharmaceutical Research, 2002 , vol. 19, # 3 p. 286 - 291
151-10-0
1,3-二甲氧基苯
→
反应条件
32274-71-8
反应条件
1: 100 percent / TiCl4 / CH2Cl2 / 0.5 h / 0 - 20 °C 2: 78 percent / DBU / benzene / 0.33 h / 80 °C 3: 94 percent / Et3N; PPh3; Pd(OAc)2 / acetonitrile / 4 h / 85 °C 4: 100 percent / MeONa / tetrahydrofuran; methanol / 1 h 5: 2 mg / EtSNa / dimethylformamide / 3 h / Heating View Scheme
参考文献
Bianco, Armandodoriano; Cavarischia, Claudia; Farina, Angela; Guiso, Marcella; Marra, Carolina
Tetrahedron Letters, 2003 , vol. 44, # 51 p. 9107 - 9110
552-41-0
丹皮酚
+
123-08-0
对羟基苯甲醛
→
反应条件
32274-71-8
反应条件
piperidine in benzene Heating;
参考文献
Gupta, Atul; Dwivedy, Anila; Keshri, Govind; Sharma, Ramesh; Balapure, Anil Kumar; Singh, Man Mohan; Ray, Suprabhat
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 23 p. 6006 - 6012
74189-56-3
4-(四氢-吡喃-2-基氧基)-苯甲醛
→
反应条件
32274-71-8
反应条件
1: partially dehydrated barium hydroxide octahydrate / ethanol / 2 h / Heating 2: 0.03 g / p-toluenesulfonic acid / methanol / 4 h / 20 °C 3: 67 percent / 10 percent H2SO4 / methanol / 7 h / Heating View Scheme
参考文献
Pouget; Fagnere; Basly; Besson; Champavier; Habrioux; Chulia
Pharmaceutical Research, 2002 , vol. 19, # 3 p. 286 - 291
123-08-0
对羟基苯甲醛
→
反应条件
32274-71-8
反应条件
1: 0.075 g / pyridinium p-toluenesulfonate / CH2Cl2 / 24 h / 20 °C 2: partially dehydrated barium hydroxide octahydrate / ethanol / 2 h / Heating 3: 0.03 g / p-toluenesulfonic acid / methanol / 4 h / 20 °C 4: 67 percent / 10 percent H2SO4 / methanol / 7 h / Heating View Scheme
参考文献
Pouget; Fagnere; Basly; Besson; Champavier; Habrioux; Chulia
Pharmaceutical Research, 2002 , vol. 19, # 3 p. 286 - 291
33527-94-5
→
反应条件
32274-71-8
反应条件
1: 94 percent / Et3N; PPh3; Pd(OAc)2 / acetonitrile / 4 h / 85 °C 2: 100 percent / MeONa / tetrahydrofuran; methanol / 1 h 3: 2 mg / EtSNa / dimethylformamide / 3 h / Heating View Scheme
参考文献
Bianco, Armandodoriano; Cavarischia, Claudia; Farina, Angela; Guiso, Marcella; Marra, Carolina
Tetrahedron Letters, 2003 , vol. 44, # 51 p. 9107 - 9110
67756-04-1
→
反应条件
32274-71-8
反应条件
1: 94 percent / Et3N; PPh3; Pd(OAc)2 / acetonitrile / 4 h / 85 °C 2: 100 percent / MeONa / tetrahydrofuran; methanol / 1 h 3: 2 mg / EtSNa / dimethylformamide / 3 h / Heating View Scheme
参考文献
Bianco, Armandodoriano; Cavarischia, Claudia; Farina, Angela; Guiso, Marcella; Marra, Carolina
Tetrahedron Letters, 2003 , vol. 44, # 51 p. 9107 - 9110
651325-80-3
→
反应条件
32274-71-8
反应条件
1: 78 percent / DBU / benzene / 0.33 h / 80 °C 2: 94 percent / Et3N; PPh3; Pd(OAc)2 / acetonitrile / 4 h / 85 °C 3: 100 percent / MeONa / tetrahydrofuran; methanol / 1 h 4: 2 mg / EtSNa / dimethylformamide / 3 h / Heating View Scheme
参考文献
Bianco, Armandodoriano; Cavarischia, Claudia; Farina, Angela; Guiso, Marcella; Marra, Carolina
Tetrahedron Letters, 2003 , vol. 44, # 51 p. 9107 - 9110
651325-79-0
→
反应条件
32274-71-8
反应条件
1: 100 percent / MeONa / tetrahydrofuran; methanol / 1 h 2: 2 mg / EtSNa / dimethylformamide / 3 h / Heating View Scheme
参考文献
Bianco, Armandodoriano; Cavarischia, Claudia; Farina, Angela; Guiso, Marcella; Marra, Carolina
Tetrahedron Letters, 2003 , vol. 44, # 51 p. 9107 - 9110
551-15-5
甘草苷
→
反应条件
32274-71-8
反应条件
1: 100 percent / methanol; diethyl ether / 1 h / 20 °C 2: 93 percent / aq. acetate buffer; β-glucosidase / 12 h / 37 °C / pH 5.0 View Scheme
参考文献
Matsuda, Hisashi; Morikawa, Toshio; Toguchida, Iwao; Yoshikawa, Masayuki
Chemical and Pharmaceutical Bulletin, 2002 , vol. 50, # 6 p. 788 - 795
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