in diethyl ether dropwise addn. of soln. of Ge-compd. to soln. of Pb-compd. with cooling to 0°C; filtered (Me3PbBr), distd.;
参考文献
Ponomarev, S. V.; Kostyuk, A. S.; Lorbert, I.; Lutsenko, I. F.
Journal of General Chemistry USSR (English Translation), 1987 , vol. 57, p. 1493 - 1494
Zhurnal Obshchei Khimii, 1987 , vol. 57, p. 1674 - 1675
methanol; triethylamine in pentane byproducts: bromotrimethylgermane; argon atmosphere; B-compd. soln. addn. to Ge-compd. soln. (stirring); B-compd. isolation on solvent and bromotrimethylgermane driving off; elem. anal.;
参考文献
Ponomarev, S. V.; Nikolaeva, S. N.; Molchanova, G. N.; Kostyuk, A. S.; Grishin, Yu. K.
Journal of General Chemistry USSR (English Translation), 1984 , vol. 54, p. 1620 - 1623
Zhurnal Obshchei Khimii, 1984 , vol. 54, p. 1817 - 1821
