4,4-二甲基二苯基二碲化物合成路线 （共 27 条）
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 38, p. 69 - 78
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 38, p. 85 - 96
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 38, p. 85 - 96
反应条件
Product distribution;
参考文献
Koellemann, Christoph; Obendorf, Dagmar; Sladky, Fritz
Phosphorus and Sulfur and the Related Elements, 1988 , vol. 38, p. 69 - 78
反应条件
sodium 1.) THF, reflux, 36 h, 2.) THF, from -20 deg C to RT; Yield given. Multistep reaction;
参考文献
Tani, Hiroyuki; Inamasu, Tokuo; Suzuki, Hitomi
Heterocycles, 1992 , vol. 34, # 2 p. 341 - 347
反应条件
1: ditolyl ditelluride With samarium; 1,2-di-iodoethane in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide T=20°C; 1 h; 2: 3,7-dimethyl-2,6-octadienyl bromide in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide T=20°C; 1.5 h; 3: 2-methyl-1,4-naphthalenedione in benzene T=100°C; 1 h; Photolysis;
参考文献
Yamago, Shigeru; Hashidume, Masahiro; Yoshida, Jun-Ichi
Tetrahedron, 2002 , vol. 58, # 34 p. 6805 - 6813
反应条件
P(pyrrolidinyl)3; [Ni(PEt3)4] in acetonitrile T=80°C; 20 h;
参考文献
Han, Li-Biao; Tanaka, Masato
Chemical Communications, 1998 , # 1 p. 47 - 48
反应条件
sodium tetrahydroborate in methanol; benzene under nitrogen, molar ratio ditelluride:Pt-complex=1:1, to dilute methanolic NaBH4 soln. was added a C6H6/MeOH (1:3, v/v) soln. of di(4-tolyl)ditelluride, benzene suspn. of Pt2Cl2(μ-Cl)2(((CH3)3C)2PC(CH3)2CH2)2 was added, stirred for 6h; solvents evapd. in vac., dissolved in C6H6, filtered off NaCl, concd. in vac., MeOH (contg. >5percent C6H6) was added, crystn. was initiated by scratching with a spatula, filtered off, washed with MeOH, dried, recrystn. from a C6H6/hexane mixt., elem. anal.;
参考文献
Jain, Vimal K.; Kannan, S.
Journal of Organometallic Chemistry, 1991 , vol. 418, # 2-3 p. 349 - 357
反应条件
sodium hydroxide; sodium tetrahydroborate in ethanol; benzene
Te adduct mixed with C6H6/EtOH, NaBH4 soln. in aq. NaOH added dropwise under reflux, Ge educt added quickly, stirred for 5 min; poured into H2O, extd. (ether), dried (Na2SO4), filtered, evapd., recrystd. (hexane); elem. anal.;
参考文献
Gerdner, S. A.; Trotter, P. J.; Gysling, H. J.
Journal of Organometallic Chemistry, 1981 , vol. 212, # 1 p. 35 - 42
反应条件
copper diacetate in water; dimethyl sulfoxide
12 h; Inert atmosphereReflux;
参考文献
Stefani, Helio A.; Pena, Jesus M.; Manarin, Flavia; Ando, Romulo A.; Leal, Daiana M.; Petragnani, Nicola
Tetrahedron Letters, 2011 , vol. 52, # 34 p. 4398 - 4401
